Triethylene Glycol Ester Plasticizer for PVC Cling Film

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Solution Overview

Problem

Existing plasticizer compositions for polyvinyl chloride resins, such as single-component and multi-component esters, fail to achieve desired properties of low heating loss, adhesiveness, and plasticization efficiency, particularly in cling film applications, due to miscibility issues and varying properties based on the type and composition of carboxylic acid and alcohol used.

Innovation Solution

A triethyleneglycol based compound and a plasticizer composition are developed, represented by specific ester formulas, which are synthesized by reacting triethyleneglycol with C3-C12 aliphatic and C6-C10 aromatic acids, along with a catalyst, to enhance miscibility and achieve improved properties like low heating loss, adhesiveness, and plasticization efficiency in polyvinyl chloride resins.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If single-component triethyleneglycol ester is used as plasticizer, then workability is improved, but miscibility with polyvinyl chloride resin decreases and transparency is reduced

Engineering Contradiction:
ImproveworkabilityVSAvoidmiscibility
Core Design Contradiction:
Ease of operationVSStability of the object's composition

Solution Approach 1:

The patent applies composite materials by combining multiple triethyleneglycol ester components with different fatty acid chains (e.g., C8-C12 medium-chain and C14-C18 long-chain esters) to create a plasticizer composition that achieves both good miscibility with PVC and desirable workability, resolving the contradiction between single-component simplicity and multi-component performance

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If single-component triethyleneglycol ester is used as plasticizer, then manufacturing simplicity is maintained, but adhesion and elongation properties deteriorate

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidadhesion and elongation
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The patent merges multiple triethyleneglycol ester components with different chain lengths and properties into a single plasticizer composition, combining the benefits of each component to achieve both manufacturing feasibility and superior adhesion and elongation properties that single components cannot provide

Inventive Principle:
Principle #5Merging (Combining)

3Adaptability or versatility

If conventional plasticizer compositions are used, then general plasticization is achieved, but heating loss increases and adhesion deteriorates

Engineering Contradiction:
Improveplasticization capabilityVSAvoidheating loss
Core Design Contradiction:
Adaptability or versatilityVSLoss of energy

Solution Approach 1:

The patent changes the chemical parameters of the plasticizer by using triethyleneglycol ester structures with specific fatty acid compositions (medium and long-chain combinations), which alters the thermal and adhesive properties to reduce heating loss while maintaining plasticization capability, addressing the limitations of conventional plasticizers

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The triethyleneglycol based plasticizer composition results in polyvinyl chloride resins with lower heating loss, excellent adhesion, higher plasticization efficiency, and improved transparency, making them suitable for food packaging applications like cling film.

Implementation Method 1

reacting triethyleneglycol with C3-C12 aliphatic and C6-C10 aromatic acids, along with a catalyst

Methodology Applied
Scientific EffectEsterification reaction: Chemical Bonding

Data Source

PatentUS7326804B2Triethyleneglycol ester based plasticizer composition for polyvinyl chloride resin and method of preparing the same
Publication Date: 2008.02.05 LG CHEM LTD

AI summary

Provided is a novel triethyleneglycol based compound, a plasticizer composition for polyvinyl chloride resin including the same, and a method of preparing the plasticizer composition. In particular, the plasticizer composition for polyvinyl chloride resin includes the novel compound, 2-(2-(2-(2-ethylhexanoyloxy)ethoxy)ethoxy)ethyl 2-ethylhexanoate, and 2-(2-(2-phenylcarbonyloxyethoxy)ethoxy)ethyl benzoate in a proper mixture ratio. A polyvinyl chloride prepared using the plasticizer composition has low heating loss, excellent adhesion, high plasticization efficiency, high elongation, high tensile strength, and high transparency.