Two-Chamber Drying System for Polyolefin Powders

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Solution Overview

Problem

Fluidized bed drying methods face challenges with non-fluidizable wet cakes that can plug openings, reduce heating efficiency, and require frequent cleaning, especially when high temperatures are not suitable for all powders, and recirculation decreases throughput.

Innovation Solution

A method involving a two-chamber drying system with back-mixing chambers and recirculation of dried powder to gradually reduce diluent concentration, using a conveyor to transfer powder between chambers, and controlled heating to achieve efficient drying of polyolefin powders with varying diluent concentrations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If fluidized bed drying is used, then drying uniformity is improved, but system reliability deteriorates due to plugging and frequent cleaning requirements

Engineering Contradiction:
Improvedrying uniformityVSAvoidsystem reliability
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The drying system is divided into multiple drying chambers (first drying chamber, second drying chamber, and optionally third drying chamber) arranged in series. Each chamber operates independently with its own heating element and gas flow system, allowing continuous drying without interruption from plugging issues in any single chamber.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A back-mixing chamber is introduced as an intermediary between the drying chambers and the fluidized bed. This back-mixing chamber receives powder from the drying chambers and feeds it to the fluidized bed, acting as a buffer that prevents direct plugging of the fluidized bed while maintaining drying uniformity.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If recirculation of material is used to fluidize non-readily fluidizable feed, then fluidization is improved, but productivity deteriorates due to decreased throughput

Engineering Contradiction:
Improvefluidization capabilityVSAvoidthroughput
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The system segments the drying process into multiple stages with separate chambers, allowing fresh powder to progress through each chamber sequentially without requiring recirculation. This maintains high throughput while achieving complete fluidization at each stage.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The back-mixing chamber performs preliminary mixing and preparation of the powder before it enters the fluidized bed. This preliminary action ensures the powder is properly conditioned for fluidization, eliminating the need for recirculation to achieve fluidization.

Inventive Principle:
Principle #10Preliminary action

3Productivity

If high temperature drying is used, then drying efficiency is improved, but adaptability deteriorates for temperature-sensitive powders

Engineering Contradiction:
Improvedrying efficiencyVSAvoidadaptability to different powders
Core Design Contradiction:
ProductivityVSAdaptability or versatility

Solution Approach 1:

Each drying chamber has its own independent heating element and gas flow control system, allowing different temperature profiles to be applied in different chambers. This enables high temperature drying in later chambers while maintaining lower temperatures in earlier chambers for temperature-sensitive materials.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The system allows dynamic adjustment of temperature and gas flow parameters in each chamber independently. This dynamic control enables adaptation to different powder types and sensitivity requirements while maintaining overall drying efficiency through optimized multi-stage processing.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method ensures uniform drying, reduces system stoppages, maintains heating efficiency, and allows for the processing of powders that are not easily fluidizable, while minimizing the need for frequent cleaning and optimizing throughput.

Implementation Method 1

a first amount of the diluent is removed from the mixture after passage through the first drying chamber

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

heating the mixture by a first heating element to a first temperature in a first gas flow

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 3

heating the mixture by a first heating element to a first temperature in a first gas flow introduced through a first gas inlet and discharged through a first gas outlet

Methodology Applied
Scientific EffectConvection: Convection

Data Source

PatentUS10788262B2Process for the preparation of a dried powder
Publication Date: 2020.09.29 BASELL POLYOLEFINE GMBH
  • US10788262B2 patent drawing
  • US10788262B2 patent drawing

AI summary

A method for preparing a dried powder is provided. The facility includes a first drying chamber having a heating element and a second drying chamber. A mixture of powder and diluent is introduced into the first drying chamber. A pre-dried powder is transferred from the first drying chamber into the second drying chamber. A dried powder, including a recirculated amount of powder and a discharge amount of powder, is formed in the second drying chamber. The recirculated amount of the dried powder is transferred by a conveyor device from the second drying chamber into the first drying chamber. The discharge amount of the dried powder is discharged from the second drying chamber.