Two-Salt Thermolytic Process for CO2 Sequestration

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Solution Overview

Problem

Current methods for carbon dioxide sequestration from power plant waste streams are energy-intensive and not economically feasible, consuming more energy than they generate, and lack efficiency in removing CO2 from flue gases.

Innovation Solution

A method involving the conversion of Group 2 silicate minerals into Group 2 chloride salts, followed by the formation of Group 2 hydroxide and/or hydroxychloride salts, which react with CO2 to form carbonate salts, utilizing heat and chemical recycling to enhance energy efficiency and reduce costs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional CO2 sequestration methods are used, then CO2 removal is achieved, but energy consumption is excessively high and economic feasibility is poor

Engineering Contradiction:
ImproveCO2 removal efficiencyVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent combines multiple process steps into an integrated cycle where CO2 capture, conversion to carbonates, and regeneration of reagents occur in a closed loop. The exothermic carbonation reaction is merged with the endothermic decomposition step, allowing heat integration that reduces external energy requirements while maintaining high CO2 removal efficiency.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent utilizes temperature and pressure parameter changes to drive the cyclic process. CO2 capture occurs at lower temperatures, while regeneration and reagent recovery occur at elevated temperatures. This parameter cycling enables the system to achieve both high CO2 removal efficiency and reduced net energy consumption by leveraging the thermodynamic properties of the chemical reactions involved.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If energy-intensive sequestration methods are employed, then CO2 is captured from flue gas, but the process consumes more energy than it generates

Engineering Contradiction:
ImproveCO2 capture effectivenessVSAvoidnet energy balance
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The patent converts the harmful CO2 emissions into a beneficial product (carbonate minerals) while simultaneously generating useful byproducts. The exothermic heat from carbonation reactions is converted into a resource that can be used for steam generation or process heating, thereby converting what would be waste heat into a useful energy source that improves the net energy balance.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The system is designed to be self-sufficient by using the heat generated from the carbonation reaction to drive the decomposition and regeneration steps. The process uses its own byproducts (heat, regenerated reagents) to sustain its operation, reducing or eliminating the need for external energy inputs and achieving a positive or neutral net energy balance.

Inventive Principle:
Principle #25Self-service

3Productivity

If existing CO2 removal techniques are implemented, then carbon sequestration is achieved, but the processes are not economically feasible

Engineering Contradiction:
Improvecarbon sequestration rateVSAvoideconomic feasibility
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The patent recovers and reuses materials that would otherwise be discarded or require continuous replenishment. The alkaline reagents are regenerated in-situ through thermal decomposition and reaction with fresh CO2, eliminating the need for continuous purchase and disposal of chemicals. This material recovery loop significantly reduces operational costs and improves economic feasibility while maintaining high carbon sequestration rates.

Inventive Principle:
Principle #34Discarding and recovering

Solution Approach 2:

The patent creates a multi-functional system that simultaneously achieves CO2 sequestration, heat generation, and reagent regeneration. The carbonate products serve both as sequestered carbon and as potential commercial products. The system processes flue gas while generating useful thermal energy and producing marketable carbonate materials, thereby improving economic feasibility through multiple revenue streams and reduced operational expenses.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively sequesters carbon dioxide into mineral carbonate form while reusing byproducts, achieving significant energy efficiency and potential profitability by utilizing inexpensive raw materials and waste heat, thereby overcoming the limitations of existing methods.

Implementation Method 1

heating a first halide or hydrate thereof with water, at least a part of which is obtained from the water of step (b), under conditions suitable to form a first product mixture comprising a first hydroxide, oxide, and/or hydroxychloride and HCl

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

admixing some or all of the first hydroxide, oxide, and/or hydroxychloride with a second halide or hydrate thereof and carbon dioxide under conditions suitable to form a second product mixture comprising a first halide or hydrate thereof, a carbonate salt, and water

Methodology Applied
Scientific EffectCarbonation reaction: Chemical Bonding

Implementation Method 3

admixing a Group 2 silicate mineral with HCl obtained from step (a), under conditions suitable to form a third product mixture comprising a Group 2 chloride, water, and silicon dioxide

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 4

These in turn may be reacted with carbon dioxide to form Group 2 carbonate salts, optionally in the presence of catalysts. These steps may be combined to form a cycle in which carbon dioxide is sequestered in the form of carbonate salts and byproducts from one or more steps, such as heat and chemicals, are re-used or recycled in one or more other steps

Methodology Applied
Scientific EffectHeat recycling: Heat Exchanger

Data Source

PatentEP2590729B1Carbon dioxide sequestrations involving two-salt-based thermolytic processes
Publication Date: 2021.01.27 CARBONFREE CHEMICALS HOLDINGS LLC
  • EP2590729B1 patent drawingFigure 1
  • EP2590729B1 patent drawingFigure 2
  • EP2590729B1 patent drawingFigure 3

AI summary

The present invention relates to an energy efficient carbon dioxide sequestration processes whereby Group 2 silicate minerals and CO2 are converted into limestone and sand using a two-salt thermolytic process that allows for the cycling of heat and chemicals from one step to another.