Two-Stage SCR Catalyst for NOx Reduction with Propylene

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Solution Overview

Problem

Current methods for reducing nitrogen oxides (NOx) emissions from combustion processes, such as those in petroleum and petrochemical refining, are expensive and have limited efficiency, necessitating an improved selective catalytic reduction technique.

Innovation Solution

A method involving a two-stage catalytic process using a first catalyst with alumina loaded with silver and a second catalyst with zirconia loaded with metals like copper, cerium, or tungsten, where a low molecular weight hydrocarbon like propylene is used as a reductant to reduce NOx emissions, with operating conditions optimized for temperature and flow rates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-generated harmful factors

If conventional SCR methods using ammonia or urea are used, then NOx reduction is achieved, but operating costs increase and efficiency is limited

Engineering Contradiction:
ImproveNOx emissionsVSAvoidremoval efficiency
Core Design Contradiction:
Object-generated harmful factorsVSProductivity

Solution Approach 1:

The patent changes the chemical parameter by substituting the reductant from ammonia/urea to propylene, and changes the catalyst composition parameter by using alumina loaded with silver and zirconia loaded with metals. This parameter change achieves higher NOx removal efficiency (>90%) while reducing operating costs, as propylene is a byproduct in petroleum refining and the new catalyst system demonstrates superior activity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite catalyst materials: alumina loaded with silver and zirconia loaded with metals (such as copper, cerium, or tungsten). These composite materials work synergistically to achieve high NOx conversion efficiency, with the alumina-silver catalyst facilitating the primary reduction and the zirconia-metal catalyst enhancing the overall performance and stability

Inventive Principle:
Principle #40Composite materials

2Object-generated harmful factors

If conventional SCR methods using ammonia or urea are used, then NOx reduction is achieved, but operating costs increase

Engineering Contradiction:
ImproveNOx emissionsVSAvoidoperating cost
Core Design Contradiction:
Object-generated harmful factorsVSLoss of energy

Solution Approach 1:

The patent enables the refining process to use its own byproduct (propylene) as the reductant for NOx removal. This self-service approach eliminates the need to purchase external reductants like ammonia or urea, thereby reducing operating costs while maintaining effective NOx control in petroleum refining operations

Inventive Principle:
Principle #25Self-service

3Object-generated harmful factors

If a two-stage catalytic process is used, then NOx removal efficiency increases, but device complexity increases

Engineering Contradiction:
ImproveNOx emissionsVSAvoidcatalyst system complexity
Core Design Contradiction:
Object-generated harmful factorsVSDevice complexity

Solution Approach 1:

The patent divides the NOx reduction process into two sequential catalytic stages: first stage using alumina loaded with silver, and second stage using zirconia loaded with metals. This segmentation allows each catalyst to perform its specific function optimally, achieving >90% overall NOx removal efficiency while maintaining manageable system complexity through modular design

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach achieves NOx reduction of greater than 90%, addressing the inefficiencies and costs of existing methods by effectively converting NOx to diatomic nitrogen and water.

Implementation Method 1

A portion of the exhaust stream and a reductant stream including a low molecular weight hydrocarbon are introduced to a first catalytic reactor, which comprises a first catalyst including alumina loaded with silver. The reductant stream and the portion of the exhaust stream being introduced to the first catalytic reactor are at suitable operating conditions to reduce the amount of NOx in the exhaust stream.

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

The NOx-reduced exhaust stream from the first catalyst is then directed to a second catalyst including zirconia loaded with at least one metal.

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

SCR is a catalytic technique to convert NOx to diatomic nitrogen, N2, and water, H2O. The low molecular weight hydrocarbon is propylene.

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 4

The first catalytic reactor can be maintained at an operating temperature between about 300°C and 400°C by heating or cooling the exhaust stream.

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentEP2882519B1Catalytic reduction of NOX with high activity catalysts with propylene reductant
Publication Date: 2020.02.12 EXXONMOBIL TECHNOLOGY & ENGINEERING CO
  • EP2882519B1 patent drawingFigure 1
  • EP2882519B1 patent drawingFigure 2A~2B

AI summary

Methods and systems are provided for selective catalytic reduction of NOx with a low molecular low molecular weight hydrocarbon, e.g., propylene, as a reductant using a catalyst system including two catalysts. An exhaust stream containing an amount of NOx from a combustion operation is provided. A portion of the exhaust stream and a reductant stream including a low molecular weight hydrocarbon is introduced to a first catalytic reactor, which comprises a first catalyst including alumina loaded with silver. The NOx-reduced exhaust stream from the first catalyst is then directed to a second catalyst including zirconia loaded with at least one metal.