Type II Cellulose Fine Fiber Processing Without Chemical Defibration

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Solution Overview

Problem

Existing methods for producing cellulose fine fibers require chemical defibration, leading to complex processes, limited applications, safety, and environmental concerns due to the use of chemical agents.

Innovation Solution

A manufacturing method involving mercerization, depolymerization, defibration using alkali metal hydroxide, and neutralization to produce type II unmodified cellulose fine fibers, which are chemically unmodified and have high transparency and safety.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of moving object

If chemical defibration is used to obtain cellulose fine fibers with small fiber diameter, then the fiber diameter is reduced, but the process complexity increases and chemical safety concerns arise

Engineering Contradiction:
Improvefiber diameterVSAvoidprocess complexity
Core Design Contradiction:
Length of moving objectVSDevice complexity

Solution Approach 1:

The patent changes the fundamental parameter of the defibration approach from chemical to physical/mechanical methods. By using mechanical energy input (mixing, shearing) instead of chemical agents, the process achieves fiber diameter reduction without introducing chemical complexity or safety concerns. The physical defibration process maintains simplicity while achieving the desired fiber size reduction.

Inventive Principle:
Principle #35Parameter changes

2Length of moving object

If chemical agents are used for defibration, then fiber diameter is reduced, but safety and environmental burden increase

Engineering Contradiction:
Improvefiber diameterVSAvoidsafety and environmental burden
Core Design Contradiction:
Length of moving objectVSObject-affected harmful factors

Solution Approach 1:

The patent replaces the chemical system with a mechanical system for defibration. Instead of using chemical agents to break down cellulose structures, the invention employs mechanical energy through mixing and shearing forces to achieve fiber separation and diameter reduction. This substitution eliminates the safety and environmental burden associated with chemical agents while maintaining the effectiveness of fiber size reduction.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Quantity of substance

If chemical defibration is employed, then cellulose fine fibers are obtained, but the number of process steps increases

Engineering Contradiction:
Improvecellulose fine fiber productionVSAvoidnumber of process steps
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The patent extracts and eliminates the chemical treatment steps from the defibration process. By removing the chemical agent addition, reaction, and removal steps, the process is simplified to focus on the essential mechanical defibration action. This extraction of unnecessary chemical steps reduces the total number of process steps while maintaining the ability to produce cellulose fine fibers effectively.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method efficiently produces chemically unmodified cellulose fine fibers with high transparency and safety, suitable for a wide range of applications, including cosmetics, and serves as an alternative to plastic products.

Implementation Method 1

a defibration step of defibrating the raw cellulose by adding an alkali metal hydroxide so as to achieve a total concentration of 2.5 to 17.5%

Methodology Applied
Scientific EffectDefibration:

Implementation Method 2

a neutralization step of neutralizing the cellulose fine fiber with an acid

Methodology Applied
Scientific EffectNeutralization:

Implementation Method 3

a mercerization step of mercerizing a cellulose to obtain a mercerized cellulose

Methodology Applied
Scientific EffectMercerization:

Data Source

PatentUS20250127704A1Type ii unmodified cellulose fine fiber and manufacturing methods for type ii unmodified cellulose fine fiber and molded body of the same
Publication Date: 2025.04.24 FUTAMURA CHEM CO LTD
  • US20250127704A1 patent drawing

AI summary

There is provided a manufacturing method for a type II unmodified cellulose fine fiber to obtain a cellulose fine fiber via mercerization of a cellulose, wherein a chemically unmodified cellulose fine fiber can be efficiently obtained by simple steps.A manufacturing method for a type II unmodified cellulose fine fiber is characterized as comprising: a mercerization step of mercerizing a cellulose to obtain a mercerized cellulose; a depolymerization step of reducing a degree of polymerization of the mercerized cellulose to 760 or less to obtain a raw cellulose; a defibration step of defibrating the raw cellulose by adding an alkali metal hydroxide so as to achieve a total concentration of 2.5 to 17.5% to obtain a cellulose fine fiber; and a neutralization step of neutralizing the cellulose fine fiber with an acid.