Urea Reactor Light Phase Distributor Design

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Solution Overview

Problem

Traditional urea synthesis reactors face inefficiencies due to non-uniform distribution of reagents, particularly carbon dioxide, which limits reaction kinetics and results in unused reactor volume, as the vertical arrangement of distributors leads to poor contact between the light and heavy phases.

Innovation Solution

A urea synthesis reactor design featuring a light phase distributor with tubular elements and intake holes distributed transversely across the reactor's cross-section, and a heavy phase distributor oriented downwards to ensure uniform distribution of carbon dioxide and ammonia/ammonium carbamate, enhancing mixing and reaction efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If vertical distributors are used in traditional urea synthesis reactors, then the construction is simpler, but the distribution of reagents (especially carbon dioxide) becomes non-uniform, limiting reaction kinetics and leaving reactor volume unused

Engineering Contradiction:
Improvereaction kineticsVSAvoiddistributor arrangement
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The light phase distributor is segmented into multiple tubular elements arranged radially across the reactor cross-section, each with intake holes distributed around its circumference. This segmentation allows carbon dioxide to be introduced at multiple locations simultaneously, achieving uniform distribution across the entire reactor cross-section and maximizing reaction kinetics throughout the volume.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention transitions from a vertical single-point injection approach to a radial multi-dimensional distribution system. The tubular elements extend radially outward from the central axis, with intake holes positioned at various angles and heights, creating a three-dimensional distribution pattern that uniformly disperses carbon dioxide throughout the reactor cross-section.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If reagents are fed through bottom distributors, then the feed system is established, but carbon dioxide forms a vertical column above the distributor, strongly limiting reaction kinetics

Engineering Contradiction:
Improvereaction kineticsVSAvoidcarbon dioxide distribution pattern
Core Design Contradiction:
ProductivityVSShape

Solution Approach 1:

Instead of injecting carbon dioxide from the bottom upward through vertical distributors, the invention inverts the approach by introducing light phase through radially arranged tubular elements that extend horizontally across the reactor cross-section. This inversion transforms the vertical column formation into a radial distribution pattern, ensuring uniform carbon dioxide dispersion throughout the reactor volume.

Inventive Principle:
Principle #13The other way round (Inversion)

Solution Approach 2:

The tubular elements are positioned at specific radial locations and angles to create locally optimized injection points. Each tubular element has intake holes positioned to target specific regions of the reactor, ensuring that carbon dioxide is distributed uniformly across the entire cross-section rather than concentrating in a vertical column above a single bottom distributor.

Inventive Principle:
Principle #3Local quality

3Productivity

If the light phase is not uniformly distributed, then construction is simpler, but part of the reactor volume remains unused due to poor contact between phases

Engineering Contradiction:
Improvereactor volume utilizationVSAvoiddistributor configuration
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The distributor system is segmented into multiple tubular elements with intake holes distributed around each tube's circumference. This segmentation enables the light phase to be introduced at numerous locations across the reactor cross-section, ensuring uniform distribution and maximizing the utilization of the entire reactor volume for the synthesis reaction.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design achieves better and more rapid mixing of reagents, leading to improved reaction efficiency and utilization of the reactor volume, with smaller carbon dioxide bubbles forming, thus increasing overall process efficiency.

Implementation Method 1

The at least one tubular element defines a plurality of spaced apart intake holes, wherein the light phase distributor is configured to distribute a light phase containing carbon dioxide to a plurality of intake points distributed transversely in the casing about the axis

Methodology Applied
Scientific EffectGas distribution through perforated tubes:

Implementation Method 2

the tube portion extends downwards towards the dome-shaped bottom portion of the casing

Methodology Applied
Scientific EffectGravitational flow: Gravitation

Implementation Method 3

This design achieves better and more rapid mixing of reagents, leading to improved reaction efficiency and utilization of the reactor volume

Methodology Applied
Scientific EffectPhase mixing:

Data Source

PatentUS10486130B2Urea synthesis reactor and process
Publication Date: 2019.11.26 SAIPEM SPA
  • US10486130B2 patent drawing
  • US10486130B2 patent drawing
  • US10486130B2 patent drawing

AI summary

A urea synthesis reactor is provided that comprises a casing extending along an axis and a first and a second inlet tube inserted through respective through openings of the casing and respectively connected, inside the casing, to a light phase distributor and to a heavy phase distributor configured to feed the reactor with a light phase containing carbon dioxide and a heavy phase containing ammonia, respectively; the light phase distributor comprises one or more tubular elements extending and/or distributed over the cross-section of the reactor and about the axis and provided with intake holes spaced apart from one another, so as to distribute said light phase in a plurality of intake points distributed transversely in the reactor and about the axis.