Urethane Resin Ink for Ejection Stability and Highlighter Resistance

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Solution Overview

Problem

Pigment inks used in inkjet recording methods suffer from low highlighter resistance and irregular ejection stability due to the adhesion of urethane resin to the recording head, leading to poor image quality and ejection accuracy.

Innovation Solution

An aqueous ink with a urethane resin having a polyether polyol unit and acidic groups, where the acid value is between 40-140 mg KOH/g and the molar ratio of urethane bonds to urea bonds is 80.0/20.0 or more, is neutralized with an alkali metal ion and ammonium type ion, maintaining a neutralization ratio of 80% or more for acidic groups and 1-45% for ammonium type ions, to enhance stability and prevent adhesion.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If urethane resin is added to pigment ink to improve highlighter resistance, then highlighter resistance is improved, but ejection stability and ejection accuracy deteriorate due to adhesion to the recording head

Engineering Contradiction:
Improvehighlighter resistanceVSAvoidejection stability
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent applies parameter changes by precisely controlling the acid value of the urethane resin (30-150 mg KOH/g) and the molar ratio of urethane bonds to urea bonds (80:20 or more). These parameter adjustments optimize the balance between highlighter resistance and ejection stability, preventing adhesion to the recording head while maintaining image fastness.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by combining urethane resin with specific chemical characteristics (acidic groups, polyether polyol units) with pigment particles. This composite approach creates an ink formulation that achieves both highlighter resistance through the urethane resin and prevents adhesion through the controlled acid value and bond ratio.

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If urethane resin with high urea bond content is used to improve highlighter resistance, then highlighter resistance is improved, but irregular ejection occurs due to adhesion to the ejection orifice surface

Engineering Contradiction:
Improvehighlighter resistanceVSAvoidejection accuracy
Core Design Contradiction:
Object-affected harmful factorsVSManufacturing precision

Solution Approach 1:

The patent applies parameter changes by setting the molar ratio of urethane bonds to urea bonds at 80:20 or more. This specific parameter control reduces the urea bond content, thereby minimizing adhesion to the ejection orifice surface and preventing irregular ejection, while still maintaining sufficient highlighter resistance through the urethane resin structure.

Inventive Principle:
Principle #35Parameter changes

3Object-affected harmful factors

If ink is stored for extended periods, then highlighter resistance is maintained, but irregular ejection develops over time due to progressive adhesion

Engineering Contradiction:
Improvehighlighter resistanceVSAvoidejection stability over time
Core Design Contradiction:
Object-affected harmful factorsVSDuration of action of stationary object

Solution Approach 1:

The patent applies preliminary action by pre-adjusting the acid value and neutralization ratio during ink formulation. This preliminary optimization prevents adhesion issues from developing during storage, ensuring that ejection stability is maintained throughout the ink's shelf life and usage period.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent uses feedback by establishing specific parameter ranges (acid value 30-150 mg KOH/g, neutralization ratio 80% or more) that are optimized based on observed adhesion behavior. These feedback-driven parameter specifications ensure long-term ejection stability by preventing the progressive adhesion that occurs with extended storage.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ink achieves improved highlighter resistance and sustained ejection stability over time, reducing irregular ejections and maintaining accurate ink droplet direction, resulting in higher-quality images.

Implementation Method 1

The acidic groups in the urethane resin are neutralized with an alkali metal ion and at least one ammonium type ion selected from ammonium ion and an organic ammonium ion

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Data Source

PatentUS9499704B2Ink, ink cartridge, and ink jet recording method
Publication Date: 2016.11.22 CANON KK

AI summary

An aqueous ink for ink jet contains a urethane resin. The urethane resin has a unit derived from a polyether polyol and a unit containing an acidic group. The acid value of the urethane resin is 40 to 140 mg KOH/g. The molar ratio of urethane bonds/urea bonds is 80.0/20.0 or more. Some of the acidic groups in the urethane resin are neutralized with particular neutralizing agents.