Vacuum Cell for Hygroscopic Optical Crystals

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Hygroscopic optically nonlinear crystals used in laser systems face degradation due to water vapor exposure, leading to reduced transparency and beam quality, and existing protection methods like coatings and hermetically sealed cells face issues with sealing reliability and laser radiation damage.

Innovation Solution

A vacuum cell with pressed-metal gas-tight gaskets and a design that separates the input and output windows from the optically nonlinear crystal, using indium gaskets for a robust seal and minimizing exposure to potential damage, while maintaining a controlled environment to prevent contamination.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If the component temperature is maintained higher than the surrounding temperature, then the polished surfaces are protected from water vapor degradation, but a controlled heat source and power supply are required

Engineering Contradiction:
Improveprotection from water vapor degradationVSAvoidheat source and power supply requirements
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent extracts the crystal from the humid environment by sealing it in a vacuum-tight cell, removing the need for thermal protection mechanisms. The crystal is isolated in a vacuum environment where water vapor cannot reach it, eliminating the requirement for heated elements while maintaining protection from degradation.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent creates an inert vacuum environment inside the cell to protect the hygroscopic crystal. By evacuating the cell to high vacuum and sealing it with vacuum-tight windows, the crystal is surrounded by an inert atmosphere free of water vapor, preventing hygroscopic degradation without requiring thermal control.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Reliability

If the surfaces are coated with a transparent, water-impermeable barrier coating, then protection from water vapor is achieved, but edge-chipping, cracking, or crazing occurs during temperature cycling and the coating degrades under intense laser light

Engineering Contradiction:
Improveprotection from water vaporVSAvoidcoating integrity under temperature cycling and laser exposure
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

Instead of applying a protective coating to the crystal surfaces, the patent extracts the crystal from the harmful humid environment by sealing it in a vacuum cell. This eliminates the need for barrier coatings that would otherwise be required to prevent water vapor contact, avoiding all the associated problems of coating failure.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a vacuum-tight cell with sealed windows as an intermediary barrier between the hygroscopic crystal and the humid external environment. This intermediary structure provides water vapor protection without requiring direct coating of the crystal surfaces, avoiding coating-related failures.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If hermetically sealed cells with robust window seals are used, then protection from water vapor and contaminants is achieved, but sealing reliability and laser radiation damage remain concerns

Engineering Contradiction:
Improveprotection from water vapor and contaminantsVSAvoidsealing reliability and laser radiation damage
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent creates a high-vacuum inert environment inside the cell to protect the crystal from water vapor and organic contaminants. The vacuum-tight seal with specially treated windows maintains this inert atmosphere, providing comprehensive protection without compromising reliability.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Solution Approach 2:

The patent changes the environmental parameters inside the cell by maintaining high vacuum conditions and controlling temperature within 5-50°C range. These parameter changes optimize both the protective function and the operational performance of the crystal while minimizing harmful effects.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If mechanical methods with bulky flanged window retaining structures are used, then sealing is achieved, but the structure becomes complex and bulky

Engineering Contradiction:
ImprovesealingVSAvoidflanged window retaining structures
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges the sealing function with the window structure itself by using elastomeric seals integrated into the window assembly. This integration eliminates the need for separate bulky flanged retaining structures, achieving reliable sealing with a more compact and simpler design.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent uses thin elastomeric sealing elements (such as O-rings or gaskets) to provide the sealing function. These flexible thin-film seals replace bulky mechanical sealing structures, achieving effective sealing with minimal complexity and space requirements.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively protects the crystal from water vapor and contamination, maintaining beam quality and conversion efficiency while minimizing the risk of damage from laser radiation, with a reliable and long-lasting seal that reduces the need for additional retaining hardware.

Implementation Method 1

The interior of such a cell is preferably evacuated and arranged to remain gas-free during operation

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 2

Each of the windows is attached to the body by a gas-tight, pressed-metal gasket

Methodology Applied
Scientific EffectGas-tight sealing:

Implementation Method 3

the process of harmonic generation, wherein an appreciable fraction of the power contained in a beam of laser light having a particular wavelength and a corresponding fundamental optical frequency is shifted to a different wavelength

Methodology Applied
Scientific EffectHarmonic generation: Second Harmonic Generation

Implementation Method 4

Hygroscopic materials absorb and retain water present in the surrounding atmosphere

Methodology Applied
Scientific EffectHygroscopy: Absorption (physical)

Data Source

PatentUS7724453B2Vacuum cell for optical components
Publication Date: 2010.05.25 COHERENT INC
  • US7724453B2 patent drawing
  • US7724453B2 patent drawing
  • US7724453B2 patent drawing

AI summary

A moisture sensitive optically nonlinear crystal is enclosed in a hermetically sealed elongated vacuum cell. The vacuum cell has an input window at one end and an output window at an opposite end providing optical access to the crystal by a laser beam. The windows are attached to the cell by cold-formed, indium-metal ram-seals. In an example of the cell in which the crystal is arranged to generate UV radiation from the laser beam, the output window is located at a sufficient distance from the crystal that the flux of UV radiation incident on the output window is below the damage threshold of the window for the UV radiation.