Vacuum Separator for Polymer Melt Degassing Gas Purification

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Solution Overview

Problem

Current methods for purifying gases from polymer melt degassing, particularly in continuous production of stretched polymer films, are inefficient in removing sublimable, non-sublimable, and condensible gases, leading to residual impurities and increased energy consumption due to the need for multiple vacuum pumps and frequent maintenance.

Innovation Solution

A method and device utilizing a vacuum separator with a cooling arrangement that freezes out impurities at temperatures below their triple point, combined with a heating arrangement to liquefy and remove them, significantly reducing gas volume and energy consumption by efficiently separating and removing sublimable, non-sublimable, and condensible gases through freezing and subsequent heating, and using a mechanical purifying device for efficient scraping and removal.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional cooling methods are used to separate gases from polymer melt degassing, then separation efficiency is limited, but energy consumption increases due to the need for multiple vacuum pumps and frequent maintenance

Engineering Contradiction:
Improveseparation efficiencyVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The patent applies phase transition by cooling the exhaust gas to freeze out condensible substances. The cooling arrangement reduces the temperature of the exhaust gas below the triple point of target impurities, causing them to transition from gas phase to solid phase and deposit on the cooling surfaces. This phase transition mechanism achieves high separation efficiency (removing over 90% of disruptive substances) while reducing the gas volume by up to 95%, thereby minimizing the need for multiple vacuum pumps and reducing energy consumption.

Inventive Principle:
Principle #36Phase transitions

2Manufacturing precision

If the exhaust gas is cooled to freeze out impurities, then separation efficiency improves, but the removed substances require additional heating and removal steps

Engineering Contradiction:
Improveseparation efficiencyVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent merges the cooling arrangement and heating arrangement into a single integrated vacuum separator device. The cooling arrangement freezes out impurities on its surfaces, and the heating arrangement subsequently heats these frozen substances to melt them for removal. This combination of opposing thermal processes within one device simplifies the overall system by eliminating the need for separate freezing and melting equipment, while maintaining high separation efficiency.

Inventive Principle:
Principle #5Merging (Combining)

3Productivity

If multiple vacuum pumps are used to handle large gas volumes, then gas purification capacity increases, but maintenance frequency and operational complexity increase

Engineering Contradiction:
Improvegas purification capacityVSAvoidmaintenance frequency
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The patent uses phase transition (freezing out) to condense and remove the majority of gas volume reductions. By cooling the exhaust gas below the triple point of target impurities, over 95% of the gas volume is reduced through freezing and deposition on cooling surfaces. This dramatically reduces the volume of gas that needs to be handled by vacuum pumps, allowing a single vacuum pump to suffice instead of multiple pumps, thereby reducing maintenance frequency and operational complexity.

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves a separation efficiency of over 90% of disruptive substances, reducing the gas volume by up to 95% and extending the service life of vacuum pumps by minimizing maintenance needs, while ensuring a continuous and energy-efficient purification process.

Implementation Method 1

the exhaust gas is cooled with liquid water, or the condensed substances are heated and subsequently removed via a removal point

Methodology Applied
Scientific EffectFreezing: Freezing

Implementation Method 2

condensible, separable by freezing, and/or re-sublimable substances are separated from the supplied and to-be-purified gas by means of a cooling arrangement

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

the substances separated by means of the cooling arrangement are at least partially liquefied or softened by means of a heating arrangement and removed from the vacuum separator

Methodology Applied
Scientific EffectMelting: Melting

Data Source

PatentUS20230241531A1Cleaning gases from the degassing of polymer melts
Publication Date: 2023.08.03 BARATTI GMBH
  • US20230241531A1 patent drawing
  • US20230241531A1 patent drawing

AI summary

A method and a device for the purification of gases from the degassing of polymer melts—in particular, for the continuous further processing to form stretched polymer films. In this case, the gas to be purified is fed from a vacuum zone of a plasticizing unit, via at least one vacuum or degassing line, to a vacuum separator with a gas inlet and a gas outlet in which condensible, separable by freezing, and/or re-sublimable substances are separated from the supplied and purified gas by means of a cooling arrangement, and the separated substances are removed from the vacuum separator. By means of a heating arrangement, the substances separated by means of the cooling arrangement are at least partially liquefied or softened in the vacuum separator and removed from the vacuum separator in particular by suction.