Sample Vaporization Unit Cap Locking for Airtight GC Sealing

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Solution Overview

Problem

The existing sample vaporization units in gas chromatographs face challenges in maintaining airtightness and facilitating the attachment and detachment of the seal cap, which complicates the maintenance and operation of the units.

Innovation Solution

A sample vaporization unit design featuring a cap fixing part with an inclined groove and an elastic protrusion that slides along this groove to ensure secure sealing of the seal cap, allowing for easy attachment and detachment without the need for tools, and maintaining constant sealing properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If a conventional vaporization unit with a large heater is used, then sufficient vaporization performance is achieved, but the response time is slow and the device is large in size

Engineering Contradiction:
Improveresponse timeVSAvoidheater size
Core Design Contradiction:
SpeedVSQuantity of substance

Solution Approach 1:

The vaporization unit is divided into multiple independent heating zones (first heating zone and second heating zone) with separate heaters. This segmentation allows each heater to be smaller while collectively providing sufficient vaporization capacity, thereby reducing the response time without requiring a single large heater that would increase size and slow response.

Inventive Principle:
Principle #1Segmentation

2Speed

If the heater size is reduced to improve response time, then response speed increases, but vaporization performance deteriorates

Engineering Contradiction:
Improveresponse timeVSAvoidvaporization performance
Core Design Contradiction:
SpeedVSProductivity

Solution Approach 1:

Multiple heating zones are merged within a single vaporization unit, with each zone having its own heater. The combined heating capacity of multiple smaller heaters equals or exceeds that of a single large heater, maintaining vaporization performance while reducing the size and response time of individual heating elements.

Inventive Principle:
Principle #5Merging (Combining)

3Productivity

If a large single heater is used, then vaporization performance is maintained, but the overall device size increases

Engineering Contradiction:
Improvevaporization performanceVSAvoiddevice size
Core Design Contradiction:
ProductivityVSVolume of moving object

Solution Approach 1:

The heating system is segmented into multiple independent heating zones distributed within the vaporization unit. This segmentation allows the use of smaller heaters that occupy less space individually, reducing the overall device volume while maintaining total vaporization capacity through the combined output of multiple zones.

Inventive Principle:
Principle #1Segmentation

4Productivity

If the heater capacity is increased to improve vaporization performance, then productivity increases, but response time increases and device size increases

Engineering Contradiction:
Improvevaporization performanceVSAvoidresponse time
Core Design Contradiction:
ProductivityVSSpeed

Solution Approach 1:

The high-capacity heating requirement is met by segmenting the total heating power across multiple independent heating zones, each with its own heater. This segmentation enables faster response times because smaller heaters heat up quicker, while the combined capacity of all zones maintains high vaporization performance.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Multiple heating zones operate simultaneously and continuously, providing sustained vaporization capacity. The parallel operation of multiple zones ensures that the total heating output remains high for maintaining productivity, while each individual zone's smaller size enables faster response when activation is needed.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design enhances the ease of attaching and detaching the seal cap, improves maintenance efficiency, and ensures reliable airtightness of the sample vaporization chamber, preventing loosening of the seal cap and maintaining consistent sealing performance.

Implementation Method 1

a first heater configured to heat the first liquid to a first temperature to generate first vapor

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 2

a second heater configured to heat the second liquid to a second temperature to generate second vapor

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 3

a mixing unit configured to mix the first vapor and the second vapor to generate mixed vapor

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP3260857B1Sample vaporization unit and gas chromatograph
Publication Date: 2023.03.29 SHIMADZU CORP
  • EP3260857B1 patent drawingFigure 1
  • EP3260857B1 patent drawingFigure 2
  • EP3260857B1 patent drawingFigure 3

AI summary

A housing is provided with an internal space for accommodating an insert and a cylindrical cap attachment part provided, at the distal end surface thereof, with an opening part communicating with the internal space. An inclined groove that is inclined from the distal end side to the proximal end side of the cap attachment part along the circumferential direction of the cap attachment part is provided on the outer circumferential surface of the cap attachment part. A cap fixing part for attaching a seal cap to the cap attachment part has a cap holding part for holding the outer peripheral surface of the seal cap and an elastic part connected to the cap holding part. The elastic part is provided with a protrusion that is fit into the inclined groove of the outer peripheral surface of the cap attachment part. The cap fixing part is attached to the cap attachment part so as to be capable of being rotated so that the protrusion slides along the inclined groove on the inside of the inclined groove and has springiness that, when the protrusion reaches the end point of the inclined groove, generates elastic force that pushes the cap holding part toward the opening part side so that the seal cap seals the opening part.