Vaporizing Section Heater for Gas Detection Accuracy

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Solution Overview

Problem

Conventional methods for detecting components of substances, particularly in liquid or solid specimens, face challenges in accuracy and efficiency due to inadequate vaporization and heating techniques, leading to inefficient component detection and potential substrate contamination.

Innovation Solution

The apparatus and method involve a vaporizing section with a substrate holder, a heater for radiant heat energy, and a detector, where the substrate is heated from the reverse surface to prevent unnecessary heating through the substrate, and gaseous matter is supplied radially inward to accelerate vaporization and stabilize component feeding to the detector, with adjustable heat energy and pressure conditions for optimal detection.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the sample is heated by a heater arranged at an upstream side in a carrier gas flow direction, then the vapor is carried to the ionization/reaction region, but the vaporization efficiency is insufficient and detection accuracy is reduced

Engineering Contradiction:
Improvevaporization efficiencyVSAvoiddetection accuracy
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The heater is moved from the upstream side to the downstream side of the carrier gas flow direction, heating the sample after the carrier gas has already passed through it. This inversion of the heating position allows the carrier gas to first carry the vaporized components and then the heater ensures complete vaporization, resolving the contradiction between vaporization efficiency and detection accuracy

Inventive Principle:
Principle #13The other way round (Inversion)

Solution Approach 2:

A thermally conductive plate is introduced as an intermediary between the heater and the sample. The plate conducts heat from the heater to the sample uniformly, improving vaporization efficiency while preventing direct contact heating that could cause localized overheating and reduce detection accuracy

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If gaseous matter is supplied toward the substance in the vaporizing section, then vaporization is accelerated and component feeding is stabilized, but the substrate may be cooled by the gaseous matter

Engineering Contradiction:
Improvevaporization rateVSAvoidsubstrate temperature
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The gaseous matter is supplied locally at the vaporizing section where it is needed to accelerate vaporization, while the substrate temperature is independently controlled by the heater. This localized application of gaseous matter achieves high vaporization rate without causing substrate cooling

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The thermally conductive plate serves as a mediator that isolates the substrate from the cooling effect of supplied gaseous matter while still allowing heat transfer from the heater to the sample. This enables accelerated vaporization without substrate temperature drop

Inventive Principle:
Principle #24Intermediary (Mediator)

3Loss of energy

If radiant heat energy is used to heat the substance, then the substance is heated directly without heating the substrate, but heating efficiency may be insufficient

Engineering Contradiction:
Improvesubstrate heat lossVSAvoidheating efficiency
Core Design Contradiction:
Loss of energyVSUse of energy by moving object

Solution Approach 1:

Both radiant heating and contact thermal conduction heating are merged into a single system. The radiant heater provides direct heating of the sample without substrate heat loss, while the contact thermal conduction heater supplements heating efficiency by conducting heat through the thermally conductive plate to the sample

Inventive Principle:
Principle #5Merging (Combining)

4Adaptability or versatility

If the distance between the substrate and heat source is adjusted, then detection of various components under optimal temperature conditions is enabled, but the device complexity increases

Engineering Contradiction:
Improvedetection rangeVSAvoidadjustment mechanism complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The distance between the substrate and heat source is made dynamically adjustable rather than fixed. This allows the system to adapt to different components requiring different optimal temperature conditions, expanding detection range without requiring multiple fixed-position heating systems

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances the accuracy and efficiency of detecting components by ensuring stable vaporization and feeding of the component to the detector, preventing substrate cooling and contamination, and allowing for the detection of various components under optimal temperature conditions.

Implementation Method 1

the substance is irradiated by a radiant heat energy to be heated

Methodology Applied
Scientific EffectRadiant heat energy: Thermal Radiation

Implementation Method 2

a reverse surface of the substrate opposite to the front surface in a stacking direction in which the substance and the substrate are stacked is heated by the heat energy with a contact thermal conduction on the reverse surface

Methodology Applied
Scientific EffectContact thermal conduction: Conduction (thermal)

Implementation Method 3

heating the substance in the vaporizing section so that the component is vaporized from the substance in the vaporizing section

Methodology Applied
Scientific EffectVaporization: Evaporation

Data Source

PatentUS7364917B2Apparatus and method for detecting vaporized gas
Publication Date: 2008.04.29 HITACHI HIGH TECH SOLUTIONS CORP
  • US7364917B2 patent drawing
  • US7364917B2 patent drawing
  • US7364917B2 patent drawing

AI summary

For detecting a component of a substance (of liquid or solid) on a front surface of a substrate, the substrate with the substance thereon is transferred into a vaporizing section, the substance is heated in the vaporizing section so that the component is vaporized from the substance in the vaporizing section, the component vaporized is fed from the substance in the vaporizing section to a detecting section, and the vaporized component is detected in the detecting section.