Vibration Mechanism for Uniform ALD Coating of Particulate Matter

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Solution Overview

Problem

In atomic layer deposition (ALD) processes for coating particulate matter, existing methods face challenges in ensuring uniform coating due to agglomeration and incomplete precursor coverage, as particulate matter tends to agglomerate and precursors do not reach all surfaces effectively.

Innovation Solution

An apparatus and method that incorporate a vibration mechanism within the reaction chamber to fluidize particulate matter, combined with a vacuum chamber and precursor system, ensuring that gaseous precursors evenly coat the particulate matter by creating movement and using heating for optimal fluidization.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If particulate matter is processed in a fluidized bed to enable uniform coating, then precursor coverage is improved, but particulate matter agglomeration occurs

Engineering Contradiction:
Improvecoating uniformityVSAvoidparticulate matter dispersion
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The patent introduces a vibration mechanism that vibrates the reaction chamber or container holding the particulate matter. This mechanical vibration prevents agglomeration by keeping particles in constant motion and ensures uniform precursor coverage by exposing all particle surfaces to the gaseous precursors, thereby resolving the contradiction between coating uniformity and particle dispersion stability.

Inventive Principle:
Principle #18Mechanical vibration

2Manufacturing precision

If vibration is applied to prevent agglomeration and ensure uniform coating, then coating quality is improved, but device complexity increases

Engineering Contradiction:
Improvecoating uniformityVSAvoidapparatus structure
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The vibration mechanism serves multiple functions: it prevents particulate matter agglomeration, ensures uniform precursor coverage, and maintains particle fluidization throughout the reaction chamber. By consolidating these functions into a single mechanism, the patent minimizes the increase in device complexity while achieving improved coating quality.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Manufacturing precision

If pressurized gas is introduced to fluidize particulate matter, then coating coverage is improved, but energy consumption increases

Engineering Contradiction:
Improveprecursor coverageVSAvoidgas pressurization energy
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The patent replaces or supplements the energy-intensive pressurized gas fluidization system with a mechanical vibration mechanism. This substitution reduces energy consumption by using mechanical oscillations instead of continuous high-pressure gas flow to achieve particle fluidization and uniform precursor coverage.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves uniform coating of particulate matter by ensuring gaseous precursors reach all surfaces, preventing agglomeration and enhancing the ALD process efficiency within a controlled vacuum environment.

Implementation Method 1

a vibration mechanism for vibrating the particulate matter inside the reaction chamber

Methodology Applied
Scientific EffectVibration: Vibration

Implementation Method 2

The vibration of the particulate matter assists in fluidization so that the first and second gaseous precursors reach all over the particulate matter

Methodology Applied
Scientific EffectFluidization: Fluidisation

Implementation Method 3

The fluidization may further be assisted through heating and in a preferred embodiment of the invention at least one heater is arranged in the vacuum chamber for providing heat to the reaction chamber

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 4

In ALD applications, typically two gaseous precursors are introduced into the ALD reactor in separate stages. The gaseous precursors effectively react with the substrate surface, resulting in deposition of a single atomic layer

Methodology Applied
Scientific EffectAtomic layer deposition: Chemical Vapour Deposition

Data Source

PatentEP3475462B1An apparatus and method for processing particulate matter
Publication Date: 2022.01.12 BENEQ OY
  • EP3475462B1 patent drawingFigure 1
  • EP3475462B1 patent drawingFigure 2
  • EP3475462B1 patent drawingFigure 3

AI summary

The invention relates to an apparatus and method for processing particulate matter by exposing the particulate matter to successive surface reactions of at least a first and a second gaseous precursor according to the principles of atomic layer deposition method. The apparatus comprises a vacuum chamber (1), a reaction chamber (2) for particulate matter, the reaction chamber (2) provided inside the vacuum chamber (1), a vibration mechanism (3) for vibrating particulate matter inside the reaction chamber (2); and a precursor system (4) arranged to supply the at least first and second gaseous precursors through the reaction chamber (2) for subjecting the particulate matter to the at least first and second gaseous precursors. The method comprises the steps of supplying the at least first and second gaseous precursors through the reaction chamber (2) for subjecting the particulate matter to the at least first and second gaseous precursors, and vibrating particulate matter inside the reaction chamber (2).