Viscous Product Sterilization via Segmented Heat Treatment

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Solution Overview

Problem

The challenge is to sterilize cosmetic products containing temperature-sensitive compounds without denaturing them, as traditional heat treatment methods can alter the properties of these compounds, and existing methods are limited by the high viscosity of the products, which prohibits the use of filters and raises concerns about the safety of preservatives used for preservation.

Innovation Solution

An apparatus and method for preparing and sterilizing a viscous fluid with a temperature-sensitive compound, involving a heat treatment unit for sterilizing the viscous matrix, a sterilizing device for the compound, and a mixing unit to incorporate the compound into the matrix, using direct or indirect heating and evaporative cooling to maintain the compound's integrity, with a dosing pump to control the flow rate of the compound.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If traditional heat treatment methods are used to sterilize cosmetic products, then sterilization effectiveness is improved, but the properties of temperature-sensitive compounds are deteriorated

Engineering Contradiction:
Improvesterilization effectivenessVSAvoiddenaturation of temperature-sensitive compounds
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The sterilization process is segmented into two independent stages: (1) sterilizing the viscous matrix separately using heat treatment, and (2) adding the temperature-sensitive compound after the matrix has cooled down. This segmentation allows the matrix to receive full sterilization treatment while the sensitive compound is exposed to minimal heat, preventing denaturation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The viscous matrix is sterilized in advance before the temperature-sensitive compound is added. By completing the sterilization process beforehand and allowing the matrix to cool, the subsequent addition of the compound does not require re-heating, thus preserving the compound's thermal sensitivity while ensuring the product is already sterilized.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If filters are used to sterilize viscous products, then sterilization is achieved, but the high viscosity of the products prohibits filter usage

Engineering Contradiction:
ImprovesterilizationVSAvoidprocessability through filters
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The sterilization function is extracted from the mixing process. Instead of attempting to filter the final viscous product containing the temperature-sensitive compound, the sterilization is performed separately on the viscous matrix alone before the compound is added. This extraction allows sterilization to occur when the product is still processable, avoiding the need to force viscous material through filters.

Inventive Principle:
Principle #2Taking out (Extraction)

3Duration of action of stationary object

If preservatives are added to extend shelf life, then product preservation is improved, but harmful preservatives are banned by regulations

Engineering Contradiction:
Improveshelf lifeVSAvoidharmful preservatives
Core Design Contradiction:
Duration of action of stationary objectVSObject-affected harmful factors

Solution Approach 1:

The chemical preservation method is replaced with a physical sterilization method. Instead of using chemical preservatives to prevent microbial growth during storage, the product is physically sterilized through heat treatment of the matrix before use. This substitution eliminates the need for harmful chemical additives while achieving the same goal of extending safe shelf life.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively extends the shelf life of cosmetic products while preserving the properties of temperature-sensitive compounds, avoiding the use of harmful preservatives and ensuring efficient sterilization without denaturation.

Implementation Method 1

Heat treatment of liquid food products for the purpose of sterilization is a commonly used industrial process. To achieve rapid heating up to high temperatures, typically exceeding 100°C, steam is employed.

Methodology Applied
Scientific EffectHeat treatment: Heating

Implementation Method 2

This normally takes place by evaporative cooling, commonly referred as flash-cooling, in a vacuum chamber. During the process, the steam is released and condensed at the same time as the product is cooled down to a similar temperature it had before the heat treatment.

Methodology Applied
Scientific EffectEvaporative cooling: Evaporation

Implementation Method 3

a sterilizing device (27), fed with a temperature sensitive compound (11), ensuring the sterilization of the temperature sensitive compound (11)

Methodology Applied
Scientific EffectSterilization: Heating

Data Source

PatentEP2959919B1Apparatus and method for the preparation and sterilization of viscous products containing temperature sensitive compounds
Publication Date: 2018.09.12 SPX APV DANMARK
  • EP2959919B1 patent drawingFigure 1
  • EP2959919B1 patent drawingFigure 2
  • EP2959919B1 patent drawingFigure 3

AI summary

The invention relates to an apparatus for the preparation and sterilization of a viscous fluid (10) containing a temperature sensitive compound (11) diluted into a viscous matrix (12), characterized in that it comprises: - a heat treatment unit (15), fed with the viscous matrix (12), wherein the viscous matrix (12) is sterilized, - a mixing unit (17), fed with the sterilized viscous matrix (12) and the sterile temperature sensitive compound (11), wherein the temperature sensitive compound (11) is incorporated into the sterilized viscous matrix (12) to form the viscous fluid (10).