Waste Treatment via Anaerobic Fermentation and MAP Precipitation

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Solution Overview

Problem

Conventional methods for processing highly organically polluted residues with high mineral content from the food industry are inefficient and costly, failing to effectively recover valuable ingredients due to complex material composition.

Innovation Solution

A method involving anaerobic fermentation, magnesium ammonium phosphate (MAP) precipitation, followed by electrochemical oxidation and reverse osmosis, utilizing an EGSB reactor and MAP reactor with specific gas and chemical inputs, and nanofiltration to process waste products with high organic acid and salt content, enabling efficient recovery and reuse of valuable ingredients.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If conventional treatment processes are used for highly organically contaminated residues with high mineral content, then the treatment can be performed with simple process engineering, but the treatment reaches its limits and cannot economically process the complex material composition

Engineering Contradiction:
Improveability to process complex waste compositionVSAvoidprocess engineering complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The treatment process is divided into multiple specialized stages: anaerobic digestion for organic matter breakdown, MAP precipitation for phosphate and ammonium recovery, nanofiltration for concentration separation, electrochemical oxidation for pollutant degradation, and reverse osmosis for water purification. Each stage targets specific components of the complex waste stream, enabling comprehensive treatment that adapts to the diverse composition of the feed material.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent introduces intermediate processing steps between the anaerobic digestion and final disposal stages. Specifically, the liquid phase containing solids from anaerobic digestion undergoes MAP precipitation as an intermediate step to recover valuable nutrients before further treatment. This intermediary process enables resource recovery while managing the complexity of the overall system.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Loss of substance

If valuable components are recovered from waste products using conventional methods, then resource utilization improves, but the extraction process becomes costly and often not fully feasible

Engineering Contradiction:
Improverecovery of valuable ingredientsVSAvoidprocessing cost
Core Design Contradiction:
Loss of substanceVSEase of manufacture

Solution Approach 1:

The anaerobic digestion process automatically concentrates valuable components (ammonium, phosphate, organic matter) in the liquid phase containing solids without requiring additional energy-intensive separation equipment. The biological process itself performs the initial concentration and separation, reducing the need for costly mechanical extraction systems and enabling economical recovery of nutrients.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent changes the physical and chemical parameters of the waste stream through controlled pH adjustment and chemical addition during MAP precipitation. By optimizing these parameters, the process selectively precipitates phosphate and ammonium as struvite crystals, enabling efficient recovery of valuable nutrients at lower costs compared to conventional extraction methods.

Inventive Principle:
Principle #35Parameter changes

3Use of energy by moving object

If anaerobic digestion is used to produce biogas from waste products, then energy recovery is achieved, but the liquid phase containing solids requires additional complex treatment steps

Engineering Contradiction:
Improvebiogas productionVSAvoidnumber of treatment steps
Core Design Contradiction:
Use of energy by moving objectVSDevice complexity

Solution Approach 1:

The liquid phase containing solids from anaerobic digestion is treated through a multi-functional process train that simultaneously achieves multiple objectives: MAP precipitation recovers phosphate and ammonium as fertilizer, nanofiltration concentrates remaining pollutants, electrochemical oxidation degrades organic contaminants, and reverse osmosis produces purified water. This universal treatment approach handles diverse contaminants in one integrated system, making the additional complexity worthwhile for achieving complete resource recovery and water reuse.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

Instead of discarding the liquid phase containing solids from anaerobic digestion as waste, the patent systematically recovers valuable components at each treatment stage. MAP precipitation recovers phosphate and ammonium, nanofiltration recovers concentrated brine for potential reuse, electrochemical oxidation recovers energy through current generation, and reverse osmosis recovers purified water. This cascading recovery approach transforms what would be a waste stream into multiple valuable products.

Inventive Principle:
Principle #34Discarding and recovering

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly improves energetic and material processing efficiency, allowing for the complete utilization of waste products, producing biogas and fertilizer-grade precipitates, and achieving drinking water quality in the final liquid phase, thus reducing disposal costs and environmental impact.

Implementation Method 1

waste products with a content of at most 12 g/l of organic acids and salt contents of at most 50 g/l are first subjected to anaerobic digestion and precipitation to produce biogas

Methodology Applied
Scientific EffectAnaerobic digestion: Anaerobic Digestion

Implementation Method 2

the other portion of the resulting liquid phase containing solids is at least partially subjected to magnesium ammonium phosphate precipitation (MAP precipitation)

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 3

the remaining portion is subjected to filtration

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 4

The permeate is subsequently subjected to electrochemical oxidation

Methodology Applied
Scientific EffectElectrochemical oxidation: Electrolysis

Implementation Method 5

the anolyte is then subjected to reverse osmosis oxidation

Methodology Applied
Scientific EffectReverse osmosis: Reverse Osmosis

Data Source

PatentEP3615476B1Method and device for treating waste products
Publication Date: 2021.09.01 FRAUNHOFER GESELLSCHAFT ZUR FORDERUNG DER ANGEWANDTEN FORSCHUNG EV
  • EP3615476B1 patent drawingFigure 1

AI summary

The invention relates to the field of process engineering and concerns a method for treating waste products, as can be used for example in the treatment of low-viscosity waste products with organic acids from the milk-processing industry. The problem addressed by the present invention is that of providing a method that achieves a much better treatment and/or use of the valuable constituents of the waste products in terms of their energy and material content. The problem is solved by a method in which waste products are first made to undergo an anaerobic fermentation and precipitation to produce biogas, the liquid phase with solid fractions that is obtained is subjected to a magnesium ammonium phosphate precipitation (MAP precipitation), then the liquid phase with solid fractions obtained in the MAP precipitation is passed on for filtering, the permeate of the filtering is subsequently passed on for electrochemical oxidation, and after that the anolyte of the oxidation is made to undergo a reverse osmosis reaction and the liquid phase then obtained is passed on for further use.