Water-Based PAI Lubricating Lacquer for Low-Temperature Curing

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Solution Overview

Problem

Existing polyamideimide (PAI) bonded coatings rely on cancerogenic, mutagenic, and reprotoxic (CMR) organic solvents, which are hazardous and may be restricted, and require high thermal curing temperatures that can deform materials like aluminum, making them unsuitable for many applications.

Innovation Solution

A water-based PAI bonded coating system using a co-crosslinking agent or co-binder, such as isocyanates, blocked isocyanates, nanoparticles, epoxides, or epoxy resins, to prevent bubble formation and improve adhesion, allowing for lower baking temperatures and eliminating the need for CMR solvents.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If CMR organic solvents (NMP, NEP, DMF, DMAc) are used as solvents for PAI binder, then the PAI solution is easy to handle and coating can be applied, but the solvents are cancerogenic/mutagenic/reprotoxic substances that are hazardous and will soon no longer be permitted

Engineering Contradiction:
Improveease of handling PAI solutionVSAvoidhazardous CMR substances
Core Design Contradiction:
Ease of operationVSObject-affected harmful factors

Solution Approach 1:

The harmful CMR organic solvents are extracted and removed from the coating system entirely. The invention replaces them with water as the solvent and uses a co-crosslinking agent to achieve proper film formation and curing, thereby eliminating the harmful substances while maintaining coating functionality

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention changes the fundamental parameter of the solvent system from organic CMR solvents to water-based system. By adjusting the formulation to include co-crosslinking agents and modifying the curing process parameters, the system achieves proper coating performance without hazardous substances

Inventive Principle:
Principle #35Parameter changes

2Reliability

If high thermal curing temperatures (200-300°C for several hours) are used to cure aqueous PAI coatings, then the coating can be cured, but the component will deform due to thermal load

Engineering Contradiction:
Improvecuring of coatingVSAvoidthermal load on component
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The invention changes the curing temperature parameter from high temperatures (200-300°C) to reduced temperatures (180-230°C). The co-crosslinking agent enables proper film formation and crosslinking at these lower temperatures, preventing component deformation while ensuring reliable coating cure

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite curing system by combining PAI binder with co-crosslinking agents (isocyanates, blocked isocyanates, nanoparticles, epoxides, or epoxy resins). This composite system enables effective curing at reduced temperatures through synergistic chemical reactions

Inventive Principle:
Principle #40Composite materials

3Reliability

If conventional aqueous PAI coatings are applied and cured, then the coating can be formed, but bubbles form on the component surface during curing resulting in poor surface quality

Engineering Contradiction:
Improveformation of coatingVSAvoidsurface quality of coating
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The co-crosslinking agent acts as an intermediary that mediates the curing process to prevent bubble formation. By controlling the crosslinking reaction and film formation kinetics, it eliminates the bubble formation issue while maintaining proper coating formation

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The combination of PAI binder with co-crosslinking agents creates a composite coating system where the co-crosslinker prevents bubble formation during curing, resulting in excellent surface quality while ensuring reliable coating formation

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves excellent adhesion and wear resistance at reduced temperatures, preventing bubble formation and ensuring a high-quality surface suitable for tribological applications, with performance comparable to solvent-based systems in pin-disc tests.

Implementation Method 1

the co-crosslinking agent prevents the formation of bubbles on the component to be coated during the curing process

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 2

The use of the co-crosslinker improves adhesion on the component

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 3

a water-based, solvent-free polyaminedimide bonded coating which also contains PTFE as an aqueous latex

Methodology Applied
Scientific EffectLubrication: Lubrication

Data Source

PatentEP3083854B8Solvent-free, water-based polyamide-imide lubricating lacquer
Publication Date: 2018.10.31 KLUBER LUBRICATION MUNCHEN SE & CO KG

AI summary

The invention relates to a polyamide-imide (PAI) lubricating lacquer which is free of organic solvents, hereinafter referred to as solvent-free, water-based PAI lubricating lacquer, and to the use thereof for the coating of metallic surfaces.