Water-Indicating Paste Stability via Proton Donating Compounds

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Solution Overview

Problem

Existing water-indicating paste compositions are prone to false color changes due to trace moisture during storage and handling, leading to instability and reduced shelf life, despite previous attempts to address these issues with boron-containing compounds and other additives.

Innovation Solution

Incorporating a proton donating compound with a pKa of not more than 12, such as organic acids like nonanoic acid or dodecylbenzene sulfonic acid, into the paste composition, which is miscible with polyalkylene glycol carriers, to enhance stability and shelf life while maintaining the ability to detect aqueous liquids.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If water-indicating paste compositions are formulated with traditional moisture inhibitors (boron-containing compounds), then water tolerance is improved, but shelf life is still limited due to trace moisture penetration during manufacture and storage

Engineering Contradiction:
Improvewater toleranceVSAvoidshelf life
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent changes the chemical parameter of the moisture inhibitor from boron-containing compounds to proton donating compounds with pKa ≤ 12. This parameter change fundamentally alters the inhibition mechanism, providing superior stability against trace moisture during manufacture and storage, thereby extending shelf life while maintaining water tolerance.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The proton donating compound acts as an intermediary substance that mediates between the indicator system and trace moisture. It donates protons to neutralize trace base contaminants and prevents premature color change, while not interfering with the water detection function when aqueous liquids are present.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Measurement precision

If the paste composition is made more sensitive to detect trace water, then detection precision is improved, but false color changes occur during storage due to trace moisture

Engineering Contradiction:
Improvedetection precisionVSAvoidfalse color changes
Core Design Contradiction:
Measurement precisionVSObject-generated harmful factors

Solution Approach 1:

The proton donating compound provides preliminary anti-action by preemptively neutralizing trace base contaminants and moisture during storage. This prevents the conditions that would trigger false color changes, allowing the paste to maintain its stable color until actual water contamination occurs.

Inventive Principle:
Principle #9Preliminary anti-action

Solution Approach 2:

The patent converts the harmful effect of trace moisture into a beneficial stabilization mechanism. The proton donating compound reacts with trace moisture and base contaminants to create a stable environment, transforming what would be a source of false positives into a protective mechanism that enhances storage stability.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Duration of action of stationary object

If proton donating compounds with pKa ≤ 12 are incorporated into the paste, then shelf life and water tolerance are improved, but the composition complexity increases

Engineering Contradiction:
Improveshelf lifeVSAvoidcomposition complexity
Core Design Contradiction:
Duration of action of stationary objectVSDevice complexity

Solution Approach 1:

The patent simplifies the composition by changing the key parameter from using complex boron-containing compounds to simpler proton donating organic acids with pKa ≤ 12. This parameter change reduces composition complexity while achieving superior performance in shelf life and water tolerance.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The paste composition exhibits improved water tolerance and extended shelf life, remaining stable under humid conditions and allowing for rapid color change upon contact with aqueous liquids, effectively preventing false positives and maintaining accuracy over time.

Implementation Method 1

Incorporating a proton donating compound with a pKa of not more than 12, such as organic acids like nonanoic acid or dodecylbenzene sulfonic acid, into the paste composition

Methodology Applied
Scientific EffectProton donation:

Implementation Method 2

an indicator dye capable of changing color in the pH range between about 3 and about 11

Methodology Applied
Scientific EffectpH indicator color change:

Data Source

PatentUS20230028877A1Water-indicating paste compositions
Publication Date: 2023.01.26 ARKEMA FRANCE SA

AI summary

A visual indicating paste composition is provided which is capable of producing a detectable color change upon contact with an aqueous liquid. The paste composition includes: an indicator dye capable of changing color in the pH range between about 3 and about 11; an inorganic base capable of being converted to a more basic substance upon reaction with water; a liquid carrier (such as a polyalkylene glycol carrier); optionally, a gelling agent such as silica gel; and a proton donating compound such as a carboxylic acid or organosulfonic acid. When applied to a measuring probe, the paste composition is particularly adapted for detecting the water level in the bottom of tanks and delivery systems containing a fuel such as gasoline by producing a clear detectable color change without bleeding or run-off upon contact with an aqueous liquid. The paste composition exhibits long shelf life and improved water tolerance.