Welded Test Material Preparation for Accurate Diffusible Hydrogen Measurement

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Solution Overview

Problem

Existing methods for evaluating delayed fracture properties in metal welds lack accuracy due to variations in measured hydrogen amounts caused by blowholes with closed structures, leading to inconsistent evaluation of cracking occurrence.

Innovation Solution

A method involving blowhole position determination and processing to eliminate closed blowholes, followed by hydrogen introduction and measurement, allowing precise evaluation of diffusible hydrogen in metal welds.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional hydrogen measurement methods are used on welded specimens, then delayed fracture evaluation can be performed, but measurement accuracy deteriorates due to hydrogen accumulation in closed blowholes

Engineering Contradiction:
Improvehydrogen measurement accuracyVSAvoidhydrogen accumulation in blowholes
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The patent applies preliminary action by performing blowhole removal or opening processing before the hydrogen measurement step. This ensures that hydrogen does not accumulate in closed blowholes during the measurement process, thereby maintaining measurement accuracy. The processing is done in advance to eliminate the harmful effect before it interferes with the measurement.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent converts the harmful effect of blowholes (which trap hydrogen and cause measurement errors) into a benefit by deliberately opening or removing them. This allows hydrogen to be evenly distributed and measured accurately, transforming the previously harmful closed structure into a useful open structure that facilitates precise measurement.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Weight of moving object

If steel material strength is increased to reduce weight, then energy efficiency improves, but delayed fracture susceptibility increases due to higher hydrogen embrittlement risk

Engineering Contradiction:
Improvevehicle weightVSAvoiddelayed fracture resistance
Core Design Contradiction:
Weight of moving objectVSReliability

Solution Approach 1:

The patent replaces mechanical strength enhancement (which increases hydrogen embrittlement susceptibility) with a chemical/compositional approach by controlling hydrogen content through improved measurement and control of diffusible hydrogen. This substitution allows high-strength materials to be used while maintaining reliability through better hydrogen management.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the parameter of hydrogen content control by implementing precise measurement methods and blowhole processing. This allows the material to maintain high strength while adjusting the hydrogen parameter to prevent delayed fracture, enabling the use of high-strength materials without proportionally increasing fracture risk.

Inventive Principle:
Principle #35Parameter changes

3Strength

If weld strength is increased to match base material strength, then joint integrity improves, but hydrogen embrittlement susceptibility increases in the weld zone

Engineering Contradiction:
Improveweld strengthVSAvoidhydrogen embrittlement in weld
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent applies local quality by specifically addressing the weld zone where hydrogen embrittlement is most problematic. Through blowhole removal/opening in the weld area and precise hydrogen measurement, the patent creates localized quality control that maintains high weld strength while preventing hydrogen accumulation specifically in the vulnerable weld zone.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent converts the harmful effect of high weld strength (which increases hydrogen embrittlement susceptibility) into a benefit by implementing blowhole processing and hydrogen control measures. This transforms the previously harmful high-strength weld into a beneficial high-strength weld with controlled hydrogen content, preventing delayed fracture while maintaining joint integrity.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate measurement of diffusible hydrogen, thereby improving the evaluation of delayed fracture properties and enabling selection of suitable metal materials for specific applications.

Implementation Method 1

immersing the specimen in 0.5 mol/L sulfuric acid, allowing hydrogen to penetrate into the specimen with an electric current

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Implementation Method 2

delayed fracture refers to a phenomenon in which, when a metal material is subjected to a static load over a period of time, a brittle fracture occurs suddenly without any significant apparent plastic deformation, and herein particularly refers to a hydrogen embrittlement fracture caused by entry of hydrogen into a metal material

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP4707796A1Method for manufacturing test material, method for measuring diffusible hydrogen content, method for evaluating delayed fracture characteristic, method for selecting metal material, and method for manufacturing member
Publication Date: 2026.03.11 JFE STEEL CORP
  • EP4707796A1 patent drawingFigure 1~2(b)
  • EP4707796A1 patent drawing
  • EP4707796A1 patent drawing

AI summary

There is provided a method for producing a test material which can measure with high accuracy the amount of diffusible hydrogen in a metal material having a weld. The method for producing a test material for measuring the amount of diffusible hydrogen in a metal material having a weld, includes: a blowhole position determination step of determining the position of a blowhole in a test material, which is a metal material having a weld; and a processing step of either processing the test material so that the blowhole, whose position has been determined in the blowhole position determination step, does not have a closed structure, or removing the blowhole.