WO3-TiO2 Catalyst Resists SOx Poisoning

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Solution Overview

Problem

Existing ammonia slip catalysts are susceptible to poisoning by sulfur oxides (SOx), which affects their performance in reducing NOx emissions in exhaust gases, especially in environments with high SOx concentrations.

Innovation Solution

A catalytic article featuring a noble metal on a WO3-TiO2 support with 1 to 20 weight percent WO3, which is resistant to SOx poisoning and effectively reduces ammonia slip when used downstream of a Selective Catalytic Reduction (SCR) process, allowing for improved NOx and ammonia oxidation in exhaust gases.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional ammonia slip catalysts are used, then ammonia oxidation can occur, but the catalyst performance deteriorates due to SOx poisoning

Engineering Contradiction:
Improvecatalyst performanceVSAvoidSOx poisoning
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent introduces a protective coating layer as an intermediary between the catalyst and the harmful SOx environment. This coating acts as a barrier that allows the catalyst to function while protecting it from sulfur poisoning, thereby maintaining long-term performance in high-SOx conditions

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent modifies the catalyst's chemical or physical parameters through the protective coating, changing its interaction with SOx. The coating alters the surface properties to prevent sulfur adsorption while maintaining ammonia oxidation activity, effectively changing the catalyst's resistance parameters

Inventive Principle:
Principle #35Parameter changes

2Reliability

If high-temperature regeneration is performed frequently to maintain catalyst activity, then catalyst performance is maintained, but fuel economy deteriorates

Engineering Contradiction:
Improvecatalyst activityVSAvoidfuel economy
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The protective coating is applied in advance to prevent sulfur accumulation before it deactivates the catalyst. This preliminary protective action eliminates the need for frequent high-temperature regenerations, reducing energy loss while maintaining catalyst activity

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent converts the harmful SOx environment into a beneficial situation by using the protective coating to prevent sulfur poisoning. This allows the catalyst to operate continuously without frequent regenerations, transforming what would be a harmful condition into an opportunity for improved fuel economy

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst maintains high performance and resistance to SOx poisoning, reducing ammonia slip and NOx emissions over a broad operational temperature range, requiring less frequent high-temperature regenerations and improving fuel economy, even with high sulfur levels in the fuel.

Implementation Method 1

absorbing at least a portion of the SOx in the catalyst layer

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 2

ammonia oxidation catalyst (AMOX) oxidizing excess ammonia

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 3

wherein the catalyst layer adsorbs at least 5 g/L of the SOx

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentEP3024574B1Tungsten/titania oxidation catalyst
Publication Date: 2021.11.24 JOHNSON MATTHEY PLC
  • EP3024574B1 patent drawingFigure 1A~1B
  • EP3024574B1 patent drawingFigure 2

AI summary

A catalyst article for treating an emission gas is provided comprising (a) an oxidation catalyst comprising at least one noble metal on a WO3-TiO2 support, wherein the support contains about 1 to about 20 weight percent WO3 based on the combined weight of the WO3 and TiO2; and (b) a substrate, wherein the first and second catalyst layers are on and/or within the substrate.