Xanthene Dye Indicator for Non-Contact Curing Progress Detection

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Solution Overview

Problem

Existing indicator systems for coating processes fail to reliably display the curing progress of compositions containing isocyanate and isocyanate-reactive components without coloring the composition in the cured state, limiting their use in clear varnishes and other color-sensitive applications.

Innovation Solution

An indicator system using a dye with a xanthene skeleton, which changes color upon contact with the uncured composition and becomes colorless in the cured state, optionally applied to an inert carrier to ensure non-contact, colorless curing indication.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If indicator dyes are added to curable compositions to show curing progress, then the curing level can be indicated, but the dye colors the cured composition, precluding use in clear varnishes

Engineering Contradiction:
Improvecuring progress indicationVSAvoidcoloration of cured composition
Core Design Contradiction:
Measurement precisionVSObject-generated harmful factors

Solution Approach 1:

The patent applies parameter changes by utilizing dyes whose molecular structure and optical properties change during the curing process. The dye molecules transition from a colored state in the uncured composition to a colorless state in the cured composition, allowing curing indication without permanent coloration. This is achieved through chemical reactions that alter the dye's conjugated system or aggregation state.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs phase transitions in the dye molecules themselves, where the dye undergoes a chemical or physical transformation during curing. The dye transitions from a soluble, colored molecular form in the uncured state to an insoluble, colorless form in the cured state, enabling the indication function while eliminating the harmful coloration effect.

Inventive Principle:
Principle #36Phase transitions

2Measurement precision

If dyes are used to indicate curing in compositions curing by radical polymerization, then color change indication is achieved, but the dyes cannot be used in compositions curing by polyaddition reaction due to potential reactions with reactive components

Engineering Contradiction:
Improvecuring indicationVSAvoidapplicability to different curing mechanisms
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent introduces an intermediary substance or mechanism that mediates between the dye and the curable composition. This intermediary protects the dye from reacting with reactive components in polyaddition-curing compositions while still allowing the dye to indicate curing progress. The intermediary could be a protective group, a specific molecular structure, or a reaction mechanism that prevents unwanted side reactions.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Device complexity

If simple color change indicators are used, then the indication method is simple, but the indicators do not provide reliable non-contact detection capability

Engineering Contradiction:
Improveindication system simplicityVSAvoidnon-contact detection reliability
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The patent utilizes color changes as the primary indication mechanism, leveraging the human eye's sensitivity to color variations. The dye undergoes distinct color transitions during curing, providing reliable visual feedback without requiring complex detection equipment. This approach maintains simplicity while achieving reliability through the inherent sensitivity of optical detection.

Inventive Principle:
Principle #32Color changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system provides a reliable, non-contact method to determine the curing progress without altering the appearance of the coated surface, enabling safe further processing and increasing the efficiency of coating operations by allowing earlier subsequent steps.

Implementation Method 1

the at least one indicator dye has a first color after contact with the uncured composition and is colorless in the cured composition

Methodology Applied
Scientific EffectColor change:

Data Source

PatentEP3668914B1Indicator system
Publication Date: 2021.07.28 COVESTRO INTELLECTUAL PROPERTY GMBH & CO KG

AI summary

The invention relates to an indicator system, a method for optically displaying the progress of curing a composition, the use of colourants with a xanthene skeleton to optically display the progress of curing compositions, a kit-of-parts, and a method for increasing the clock rate between a coating step and an additional, downstream processing step for objects.