X-ray Detector Sensitivity Calibration Using Multipurpose Source

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Solution Overview

Problem

Existing X-ray diffraction analyzers require a uniform and expensive X-ray source for sensitivity correction, making it difficult for users to recalibrate the sensitivity correction coefficient in field settings, and it is challenging to determine if recalibration is necessary.

Innovation Solution

A sensitivity correction coefficient calculating system that uses a multipurpose X-ray source to fit the X-ray intensity distribution with an approximation function, allowing for the calculation of sensitivity correction coefficients for each detection element without the need for a specific X-ray source, enabling recalibration using a reference sample.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a uniform X-ray source is used for sensitivity correction, then measurement precision is improved, but device complexity and cost increase

Engineering Contradiction:
Improvesensitivity correction precisionVSAvoidX-ray source complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent uses an approximation function to create a mathematical model (copy) of the actual X-ray intensity distribution from a multipurpose source. This virtual uniform distribution allows sensitivity correction without requiring a physical uniform X-ray source, resolving the contradiction between measurement precision and device complexity

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The patent changes the approach from using a physical uniform X-ray source to using a mathematical approximation of intensity distribution. By parameterizing the intensity distribution through fitting functions, the system achieves sensitivity correction with a multipurpose source instead of requiring specialized uniform source hardware

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If a specific uniform X-ray source is required, then sensitivity correction accuracy is improved, but ease of operation deteriorates

Engineering Contradiction:
Improvesensitivity correction accuracyVSAvoidrecalibration ease
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The patent makes the sensitivity correction process universal by enabling it to be performed with a multipurpose X-ray source that can serve both analytical and calibration functions. The approximation function approach allows any X-ray source to be used for sensitivity correction, eliminating the need for specialized uniform sources and making recalibration feasible in field settings

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The system enables users to perform sensitivity correction themselves using the multipurpose X-ray source and approximation function method. This self-service capability eliminates dependence on specialized equipment and external calibration services, significantly improving ease of operation for field recalibration

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables the calculation of sensitivity correction coefficients using a multipurpose X-ray source, allowing for recalibration of X-ray detectors without the need for a uniform X-ray source, simplifying the process and making it feasible in field settings.

Implementation Method 1

characteristic X-rays generated in the target can be emitted

Methodology Applied
Scientific EffectCharacteristic X-ray emission: X-Ray

Implementation Method 2

detect the diffracted X-rays that are emitted from the powder sample

Methodology Applied
Scientific EffectX-ray diffraction: Diffraction

Implementation Method 3

detection elements for detecting the intensity of the X-rays

Methodology Applied
Scientific EffectX-ray detection: Photoelectric Effect

Data Source

PatentUS10145809B2X-ray diffraction device and sensitivity calibration method for X-ray diffraction device
Publication Date: 2018.12.04 SHIMADZU CORP
  • US10145809B2 patent drawing
  • US10145809B2 patent drawing
  • US10145809B2 patent drawing

AI summary

The invention provides a sensitivity correction coefficient calculating system for an X-ray detector with which the sensitivity correction coefficient can be calculated using a multipurpose X-ray source instead of a specific X-ray source. In the sensitivity correction coefficient calculating system for an X-ray detector having a detection surface where detection elements for detection the X-ray intensity are aligned one-dimensionally or two-dimensionally, fitting is carried out on the measured X-ray intensity detected by a detection element using an approximation function so as to calculate the sensitivity correction coefficient using the calculated X-ray intensity calculated from the approximation function and the measured X-ray intensity.