Multi-layer X-ray Grating Self-Alignment Fabrication

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Solution Overview

Problem

Current X-ray phase-contrast imaging technologies face challenges in fabricating high-resolution, multi-layer high-aspect ratio X-ray gratings for compact systems and higher energy applications, particularly due to stringent requirements for grating feature sizes and aspect ratios, which affect image quality and detail information, especially when trying to achieve larger field-of-view imaging.

Innovation Solution

A multi-layer high-aspect ratio X-ray grating fabrication method involving a seed layer, patterned non-X-ray absorbing layers, and X-ray absorbing layers, with self-alignment through backside radiation exposure, such as UV, EUV, or IR exposure, using materials like gold, platinum, or indium, and a combination of SU-8 photoresist and LIGA processes to create periodic structures for improved alignment and aspect ratio.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional single-layer grating fabrication methods are used, then manufacturing process is simpler, but manufacturing precision and aspect ratio are insufficient for high-resolution imaging

Engineering Contradiction:
Improvegrating feature size and aspect ratio precisionVSAvoidfabrication process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The grating structure is divided into multiple layers, with each layer containing alternating absorbing and non-absorbing regions. This segmentation allows achieving high aspect ratios and precise feature sizes by stacking multiple simpler patterns rather than attempting to fabricate a single complex high-aspect-ratio structure in one step.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The fabrication approach transitions from two-dimensional planar patterns to three-dimensional multi-layer stacked structures. By adding the vertical dimension through multiple stacked layers, the grating achieves high aspect ratios while maintaining precise lateral feature sizes defined by the underlying 2D patterns.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Manufacturing precision

If alignment precision is increased to improve imaging quality, then image quality improves, but alignment process complexity and difficulty increase

Engineering Contradiction:
Improvealignment accuracy between grating layersVSAvoidalignment measurement and control difficulty
Core Design Contradiction:
Manufacturing precisionVSDifficulty of detecting and measuring

Solution Approach 1:

The patterned non-absorbing layers serve as self-aligned alignment references for subsequent absorbing layer patterning. The self-aligned process uses the previously formed patterns as built-in alignment features, eliminating the need for external alignment measurement and control systems, thereby achieving high precision without increased operational complexity.

Inventive Principle:
Principle #25Self-service

3Measurement precision

If grating aspect ratio is increased for higher resolution, then imaging resolution improves, but mechanical stability and fabrication feasibility deteriorate

Engineering Contradiction:
Improveimaging resolutionVSAvoidgrating mechanical stability
Core Design Contradiction:
Measurement precisionVSStability of the object's composition

Solution Approach 1:

The high aspect ratio grating is segmented into multiple lower aspect ratio layers stacked vertically. Each layer maintains mechanical stability with its own patterned non-absorbing structures providing support, while collectively achieving the desired high aspect ratio. This segmentation distributes mechanical stress across multiple layers rather than concentrating it in a single high-aspect-ratio structure.

Inventive Principle:
Principle #1Segmentation

4Area of stationary object

If field-of-view is increased for larger imaging area, then imaging coverage improves, but grating fabrication area and complexity increase

Engineering Contradiction:
Improvegrating field-of-view areaVSAvoidlarge area grating fabrication complexity
Core Design Contradiction:
Area of stationary objectVSDevice complexity

Solution Approach 1:

The large area grating is divided into multiple stacked layers, each covering the same field-of-view area but with simplified individual patterns. This segmentation allows fabricating large area gratings by stacking multiple smaller, easier-to-fabricate layers rather than attempting to pattern a single large area structure, thereby reducing overall fabrication complexity.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables the production of high-resolution, high-aspect ratio X-ray gratings with improved alignment accuracy and mechanical stability, facilitating higher contrast and sensitivity in X-ray phase-contrast imaging, especially for larger field-of-view applications without the need for specialized facilities, thus enhancing imaging quality and resolution.

Implementation Method 1

fabricating the at least one patterned non-X-ray absorbing layer includes exposing the grating to backside radiation exposure

Methodology Applied
Scientific EffectPhoto-sensitive material exposure: Photopolymerisation

Implementation Method 2

at least one X-ray absorbing layer made from gold, platinum, nickel, lead, selenium, bismuth, tungsten, or indium

Methodology Applied
Scientific EffectRadiation absorption: Absorption (EM radiation)

Data Source

PatentUS20240353353A1Multi-layer high-aspect ratio x-ray grating and method of manufacture
Publication Date: 2024.10.24 KARIM KARIM S
  • US20240353353A1 patent drawing
  • US20240353353A1 patent drawing
  • US20240353353A1 patent drawing

AI summary

The disclosure is directed at a multi-layer, high-aspect ratio X-ray grating apparatus and method of fabrication. In one embodiment, the disclosure may include a self-alignment methodology, or process, combined with a multiple layer structure fabrication. The grating may include a substrate with a seed layer on top. The grating further includes at least one patterned non-X-ray absorbing layer and at least one X-ray absorbing layer atop the seed layer.