X-ray Fluorescence Analyzer Collimator Rotation

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Solution Overview

Problem

In X-ray fluorescence analysis, spatially non-uniform X-ray intensity leads to incomplete analysis of samples with non-uniformly distributed elements, necessitating uniform attenuation of X-rays.

Innovation Solution

An X-ray fluorescence analyzer with a collimator having a transmission region that increases in circumference from a vertex positioned on the axis of rotation, allowing for uniform X-ray attenuation through rotation of the sample and collimator, combined with an intensity control unit to prevent signal saturation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a collimator is used to attenuate X-rays to prevent detection signal saturation, then the detection signal saturation is prevented, but the X-ray intensity becomes spatially non-uniform

Engineering Contradiction:
Improvedetection signal saturation preventionVSAvoidspatial uniformity of X-ray intensity
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The collimator is rotated about its axis during X-ray irradiation, transforming a static non-uniform attenuation structure into a dynamic system that achieves uniform attenuation over time. The rotation allows different angular sections of the collimator to sequentially attenuate X-rays to various parts of the sample, resulting in spatially uniform effective attenuation.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The collimator performs periodic rotation during the X-ray irradiation process. This periodic motion ensures that each region of the sample receives X-rays that have been attenuated by different portions of the collimator at different times, achieving uniform attenuation distribution through repeated cyclic action.

Inventive Principle:
Principle #19Periodic action

2Reliability

If the intensity of X-rays emitted by the X-ray source is minimized to prevent detection signal saturation, then detection signal saturation is prevented, but the number of detected photons is reduced

Engineering Contradiction:
Improvedetection signal saturation preventionVSAvoidnumber of detected photons
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

Instead of simply minimizing X-ray intensity, the system changes the attenuation parameter distribution by rotating the collimator. This allows the use of higher overall X-ray intensity while maintaining uniform attenuation, thereby increasing the number of detected photons while preventing saturation.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Ensures spatially uniform X-ray attenuation and prevents detection signal saturation, enabling accurate analysis of samples with varying compositions.

Implementation Method 1

The collimator is a plate-like member having an opening and attenuates the X-rays emitted to a sample by blocking a part of the X-rays emitted from the X-ray source

Methodology Applied
Scientific EffectX-ray attenuation: Absorption (EM radiation)

Implementation Method 2

a sample is irradiated with X-rays from an X-ray source to excite the sample, so that fluorescent X-rays are released from the sample

Methodology Applied
Scientific EffectX-ray emission: X-Ray

Implementation Method 3

The number of photons per hour (hereinafter simply referred to as the 'number of photons') of the fluorescent X-rays released from the sample is detected by a detector

Methodology Applied
Scientific EffectX-ray detection: Photoelectric Effect

Data Source

PatentUS11391680B2X-ray fluorescence analyzer and X-ray fluorescence analysis method
Publication Date: 2022.07.19 SHIMADZU CORP
  • US11391680B2 patent drawing
  • US11391680B2 patent drawing
  • US11391680B2 patent drawing

AI summary

A support unit and a collimator are relatively rotated about the axis of rotation by a rotation driving device. The collimator has a blocking region that blocks X-rays and a transmission region that allows X-rays to pass therethrough. The transmission region has a vertex positioned on the axis of rotation, and the circumferential length of the transmission region increases proportionally as it advances outward from the vertex. A sample supported by the support unit is irradiated with X-rays by an X-ray source through the transmission region of the collimator, and the fluorescent X-rays from the sample are detected by the detector. The analysis of a composition of a sample is performed based on the fluorescent X-rays detected by the detector.