Grazing Incidence XRF Spectrometer Slit Mechanism

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Solution Overview

Problem

Conventional X-ray fluorescence spectrometers have complex structures due to multiple units required for adjusting X-ray sources and spectroscopic devices, leading to increased costs and complexity, which hinders high-sensitivity and high-accuracy analysis.

Innovation Solution

A grazing incidence X-ray fluorescence spectrometer with a bent spectroscopic device, a slit member, and a glancing angle setting unit that allows for automatic adjustment of the X-ray beam's angle, using a variable slit member and multilayer films to focus X-rays on a sample, enabling precise analysis with a low-cost, simple structure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If multiple units (X-ray source selection unit, X-ray source adjustment unit, spectroscopic device position adjustment unit) are provided to enable automatic adjustment and high sensitivity analysis, then analysis sensitivity and accuracy are improved, but device complexity and cost increase

Engineering Contradiction:
Improveanalysis sensitivity and accuracyVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent combines the functions of the slit member (which limits X-ray beam width) and the angle adjustment mechanism into a single integrated component. The slit member is moved by a simple moving unit to simultaneously achieve both beam width control and glancing angle adjustment, eliminating the need for separate X-ray source adjustment units and spectroscopic device position adjustment units, thus reducing device complexity while maintaining measurement precision

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The slit member serves multiple functions: it limits the width of the X-ray beam, controls the focusing angle, and through its movement, adjusts the glancing angle. This multi-functional design replaces multiple specialized units, achieving high sensitivity and accuracy analysis without increasing device complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Measurement precision

If multiple units are provided for automatic adjustment, then analysis accuracy is improved, but manufacturing cost increases

Engineering Contradiction:
Improveanalysis accuracyVSAvoidmanufacturing cost
Core Design Contradiction:
Measurement precisionVSEase of manufacture

Solution Approach 1:

The patent extracts and eliminates unnecessary complex adjustment units from the system. By using the slit member's movement to achieve angle adjustment functionality, it removes the need for separate X-ray source adjustment units and spectroscopic device position adjustment units, thereby reducing manufacturing cost while maintaining analysis accuracy through the simplified structure

Inventive Principle:
Principle #2Taking out (Extraction)

3Device complexity

If a simple structure is used to reduce cost, then device complexity is reduced, but achieving high sensitivity and accuracy becomes difficult

Engineering Contradiction:
Improvedevice complexityVSAvoidanalysis sensitivity and accuracy
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The patent achieves high sensitivity and accuracy analysis with a simple structure by precisely controlling the glancing angle parameter. The slit member is moved to set the glancing angle to an optimal value, and the beam width is controlled through the slit's positioning, enabling accurate analysis without complex multi-unit systems

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The spectrometer achieves high sensitivity and accuracy in elemental analysis and thin film thickness measurement with reduced complexity and cost, using a focused X-ray beam and adjustable glancing angle to optimize analysis conditions.

Implementation Method 1

a bent spectroscopic device configured to monochromate the X-rays emitted from the X-ray source and form an X-ray beam that is focused on a fixed position on a surface of a sample

Methodology Applied
Scientific EffectX-ray monochromatization and focusing: Bragg Diffraction

Implementation Method 2

a slit member disposed between the bent spectroscopic device and the sample, the slit member having a linear opening by which a width of the passing X-ray beam is limited in a focusing angle direction

Methodology Applied
Scientific EffectBeam width limitation:

Implementation Method 3

a slit member moving unit configured to move the slit member in a direction that intersects the X-ray beam passing through the linear opening; a glancing angle setting unit configured to move the slit member by using the slit member moving unit, and set a glancing angle of the X-ray beam to a desired angle

Methodology Applied
Scientific EffectMechanical movement for angle adjustment:

Implementation Method 4

a detector configured to measure an intensity of fluorescent X-rays generated from the sample that is irradiated with the X-ray beam

Methodology Applied
Scientific EffectX-ray fluorescence: Fluorescence

Data Source

PatentUS10302579B2Grazing incidence x-ray fluorescence spectrometer and grazing incidence x-ray fluorescence analyzing method
Publication Date: 2019.05.28 RIGAKU CORP
  • US10302579B2 patent drawing
  • US10302579B2 patent drawing
  • US10302579B2 patent drawing

AI summary

A grazing incidence X-ray fluorescence spectrometer (1) of the present invention includes: a bent spectroscopic device (4) to monochromate X-rays (3) from an X-ray source (2) and generate an X-ray beam (5) focused on a fixed position (15) on a surface of a sample (S); a slit member (6) disposed between the bent spectroscopic device (4) and the sample (S) and having a linear opening (61); a slit member moving unit (7) to move the slit member (6) in a direction that intersects the X-ray beam (5) passing through the linear opening (61); a glancing angle setting unit (8) to move the slit member (6) by using the slit member moving unit (7), and set a glancing angle (α) of the X-ray beam (5) to a desired angle; and a detector (10) to measure an intensity of fluorescent X-rays (9) from the sample (S) irradiated with the X-ray beam (5).