Yttrium-Stabilized Beta-Sialon Ceramic Cutting Tools

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Solution Overview

Problem

Existing silicon nitride ceramic materials for cutting tools lack sufficient wear resistance and toughness for machining heat-resistant super alloys, particularly when used for nickel- or cobalt-based materials at elevated temperatures.

Innovation Solution

A ceramic material composed of β-sialon (Si(6-z)AlzOzN(8-z)) and polytype 15R with intergranular phase, containing yittrium, where the polytype 15R phase includes twin grains and is present between 25% and 55% as measured by X-ray diffraction patterns.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional silicon nitride ceramic materials are used for cutting tools, then the basic cutting function is provided, but wear resistance and toughness are insufficient for machining heat-resistant super alloys

Engineering Contradiction:
Improvewear resistanceVSAvoidtoughness
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent creates a composite ceramic material consisting of β-sialon phase (40-60 wt%) providing wear resistance, polytype 15R phase (20-40 wt%) enhancing toughness through twin grain structures, and intergranular phase (10-30 wt%) containing yittrium for grain boundary strengthening. This multi-phase composite structure resolves the contradiction by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent applies local quality by creating distinct phases with specific functions: β-sialon regions provide hard wear-resistant zones, polytype 15R regions with twin grains provide toughening zones, and intergranular phases provide boundary strengthening. Each phase is optimized for its specific role to collectively improve both wear resistance and toughness.

Inventive Principle:
Principle #3Local quality

2Ease of manufacture

If aluminum oxide is used as a sintering additive to form sialon ceramic, then sintering is facilitated, but the resulting material lacks sufficient toughness for HRSA machining

Engineering Contradiction:
Improvesintering capabilityVSAvoidtoughness
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The patent changes the phase composition parameters by controlling the ratio of β-sialon to polytype 15R phases, and adjusting the content of intergranular phase containing yittrium. By optimizing these parameters (β-sialon: 40-60 wt%, polytype 15R: 20-40 wt%, intergranular phase: 10-30 wt%), the material achieves both manufacturability and enhanced toughness.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The intergranular phase containing yittrium acts as an intermediary between the β-sialon and polytype 15R phases, facilitating grain boundary bonding and stress transfer. This intermediary phase enables the composite structure to achieve both ease of manufacture through conventional sintering and improved toughness through effective stress distribution.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Strength

If the polytype 15R phase is increased to improve toughness, then fracture toughness increases, but the optimal balance with wear resistance must be maintained

Engineering Contradiction:
Improvefracture toughnessVSAvoidwear resistance
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent optimizes the weight percentage of polytype 15R phase within 20-40% to achieve the optimal balance between fracture toughness and wear resistance. This parameter optimization ensures sufficient toughness enhancement while maintaining adequate wear resistance through the complementary β-sialon phase.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ceramic material exhibits enhanced wear resistance and toughness, as demonstrated by increased fracture toughness and reduced brittleness, leading to improved performance in machining heat-resistant super alloys, with specific examples showing extended tool life during milling tests.

Implementation Method 1

the polytype 15R phase includes twin grains

Methodology Applied
Scientific EffectTwin grain strengthening: Grain Boundary Strengthening

Implementation Method 2

The ceramic material exhibits enhanced wear resistance and toughness

Methodology Applied
Scientific EffectWear resistance: Wear

Data Source

PatentEP3218323B1Ceramic material and cutting tools made thereof
Publication Date: 2019.07.31 TAEGUTEC
  • EP3218323B1 patent drawingFigure 1~2
  • EP3218323B1 patent drawingFigure 3~5
  • EP3218323B1 patent drawingFigure 6~8

AI summary

A ceramic material according to an exemplary embodiment consists of β-sialon (Si(6-z)AlzOzN(8-z)) and polytype 15R and intergranular phase, and contains yittrium, in which the polytype 15R includes twin grains.