Zinc Phosphate Oral Care Compositions for Stannous Ion Stability

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Solution Overview

Problem

Conventional oral care compositions face challenges in achieving antibacterial efficacy while maintaining palatability and avoiding the drawbacks of high zinc concentrations, astringency, and instability of stannous ions, such as stannous fluoride, which are commonly used for their antimicrobial properties.

Innovation Solution

Incorporating specific amounts of zinc phosphate and stannous pyrophosphate, along with stannous fluoride, to enhance the delivery and stability of stannous ions in oral care compositions, thereby improving antimicrobial efficacy and reducing unpleasant tastes and staining.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If high concentrations of zinc (e.g., 2% or more) are used to achieve antibacterial efficacy, then antimicrobial effectiveness is improved, but astringent taste and user acceptability worsen

Engineering Contradiction:
Improveantimicrobial effectivenessVSAvoidastringent taste
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical form of zinc from conventional soluble zinc salts to zinc phosphate (insoluble in water), and uses acidulation during brushing to convert it to soluble forms in situ. This parameter change allows achieving antimicrobial effectiveness while avoiding the astringent taste associated with high concentrations of conventional zinc salts.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces acidulants (e.g., citric acid, ascorbic acid) as intermediaries that convert insoluble zinc phosphate to soluble zinc forms during the brushing process. This intermediary mechanism enables controlled release of zinc ions at the application site, providing antimicrobial action without the need for high concentrations of pre-dissolved zinc that cause astringency.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If stannous salts (e.g., stannous fluoride) are used for plaque prevention, then antimicrobial effectiveness is improved, but stability, staining, and astringency worsen

Engineering Contradiction:
Improveplaque prevention effectivenessVSAvoidstability in aqueous solution
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent uses stannous phosphate as an insoluble reservoir that releases stannous ions gradually during brushing. This approach replaces the need for stable pre-dissolved stannous salts with a stable insoluble form that provides controlled, short-term release of active ions during the brief brushing period, avoiding stability issues while maintaining effectiveness.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent employs acidulants as intermediaries to convert insoluble stannous phosphate to soluble stannous forms during brushing. This intermediary conversion mechanism enables stable storage of stannous ions in an insoluble form while providing effective release at the application site, resolving the stability-effectiveness contradiction.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If stannous salts are used for gingivitis reduction, then therapeutic benefit is improved, but precipitation and loss of therapeutic properties worsen

Engineering Contradiction:
Improvegingivitis treatment effectivenessVSAvoidresistance to precipitation
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent uses stannous phosphate as a stable insoluble reservoir that releases stannous ions during the short duration of brushing. This approach eliminates precipitation problems associated with storing stannous ions in aqueous solution, as the ions are released in controlled amounts during use rather than being pre-dissolved and prone to precipitation over time.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent changes the solubility parameter of stannous ions by using insoluble stannous phosphate that converts to soluble forms in the acidic oral environment during brushing. This parameter change ensures stability during storage while providing effective release during use, preventing precipitation and loss of therapeutic properties.

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If low water oral care compositions are used to improve stannous ion stability, then stability is improved, but rheological properties and ease of formulation worsen

Engineering Contradiction:
Improvestannous ion stabilityVSAvoidformulation difficulty
Core Design Contradiction:
Stability of the object's compositionVSEase of manufacture

Solution Approach 1:

The patent uses insoluble stannous phosphate as a stable reservoir that requires no special low-water formulation techniques. The insoluble nature of stannous phosphate provides inherent stability without compromising the aqueous-based formulation, eliminating the need for complex low-water or dual-phase systems while maintaining ease of manufacture.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

5Stability of the object's composition

If dual phase systems are used to improve stannous ion stability, then stability is improved, but manufacturing cost and complexity worsen

Engineering Contradiction:
Improvestannous ion stabilityVSAvoidformulation complexity
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The patent uses a single-phase aqueous formulation containing insoluble stannous phosphate particles. This simple single-phase system eliminates the complexity of dual-phase systems while providing equivalent stability benefits, as the insoluble stannous phosphate naturally resists precipitation and degradation in the aqueous environment without requiring phase separation or special packaging.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The combination of zinc phosphate and stannous pyrophosphate enhances the delivery of stannous ions, providing effective antibacterial action against plaque and gingivitis while maintaining a pleasant taste and stability, thus improving oral health outcomes.

Implementation Method 1

Incorporating specific amounts of zinc phosphate and stannous pyrophosphate, along with stannous fluoride, to enhance the delivery and stability of stannous ions in oral care compositions

Methodology Applied
Scientific EffectControlled release:

Implementation Method 2

enhance the delivery and stability of stannous ions in oral care compositions, thereby improving antimicrobial efficacy and reducing unpleasant tastes and staining

Methodology Applied
Scientific EffectStability enhancement:

Implementation Method 3

providing effective antibacterial action against plaque and gingivitis while maintaining a pleasant taste and stability

Methodology Applied
Scientific EffectAntimicrobial action:

Data Source

PatentUS12419817B2Oral care compositions and methods of use
Publication Date: 2025.09.23 COLGATE PALMOLIVE CO

AI summary

This invention relates to oral care compositions comprising zinc phosphate, a first source of stannous (e.g., stannous fluoride); and a second source of stannous, wherein the second source of stannous comprises stannous pyrophosphate, as well as to methods of using and of making these compositions.