Aluminum-Free Antiperspirant Zinc Substantivity via pH Control

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Solution Overview

Problem

Current roll-on antiperspirant/deodorant products using aluminum salts face issues with erratic efficacy due to precipitation and solubility concerns, particularly with zinc salts, which have limited substantivity on the skin surface.

Innovation Solution

An antiperspirant/deodorant composition featuring an oil-in-water emulsion base with a mixture of steareth-2 and steareth-20 as emulsifiers, incorporating zinc-based actives like zinc oxide, zinc hydroxide, and film-forming polymers to enhance zinc substantivity on the skin, while being free of aluminum, magnesium, and calcium-based actives.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If zinc salts are used as antiperspirant active, then aluminum-free formulation is achieved, but zinc precipitates as hydroxides at pH 6.5-8.0 causing erratic efficacy

Engineering Contradiction:
Improvealuminum-free formulationVSAvoidefficacy consistency
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The patent changes the pH parameter of the formulation to below 6.5, which prevents zinc hydroxide precipitation and maintains zinc solubility. This pH adjustment resolves the contradiction by enabling aluminum-free formulation while ensuring consistent zinc-based antiperspirant efficacy through controlled chemical parameters.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite emulsion systems containing zinc salts combined with specific emulsifiers and co-emulsifiers that stabilize the formulation at low pH. This composite approach maintains zinc in solution while providing the desired aluminum-free antiperspirant effect with consistent performance.

Inventive Principle:
Principle #40Composite materials

2Adaptability or versatility

If zinc oxide is used as antiperspirant active, then aluminum-free formulation is achieved, but perspiration dissolves zinc oxide depositions reducing duration of action

Engineering Contradiction:
Improvealuminum-free formulationVSAvoidduration of action
Core Design Contradiction:
Adaptability or versatilityVSDuration of action of stationary object

Solution Approach 1:

The patent adjusts the pH parameter to below 6.5, which reduces the solubility of zinc oxide in perspiration. This prevents dissolution of zinc depositions and extends the duration of action while maintaining aluminum-free formulation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces emulsifiers and co-emulsifiers as intermediary substances that enhance the adhesion and substantivity of zinc oxide to the skin. These intermediaries create a more stable deposit that resists dissolution by perspiration, thereby extending duration of action.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Adaptability or versatility

If zinc salts are used to replace aluminum, then aluminum-free formulation is achieved, but zinc substantivity on skin surface is limited

Engineering Contradiction:
Improvealuminum-free formulationVSAvoidzinc substantivity
Core Design Contradiction:
Adaptability or versatilityVSQuantity of substance

Solution Approach 1:

The patent changes the pH parameter to below 6.5 and optimizes the concentration of emulsifiers and co-emulsifiers to enhance zinc substantivity. These parameter adjustments increase zinc deposition on the skin surface while maintaining aluminum-free formulation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses emulsifiers and co-emulsifiers as intermediaries that enhance zinc adhesion to the skin. These substances facilitate greater zinc substantivity by improving the interaction between zinc salts and the skin surface, thereby increasing the quantity of effective zinc deposited.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition provides increased substantivity of zinc on the skin, reducing apparent perspiration and minimizing side effects like stinging, burning, and tingling, with improved skin feel and stability.

Implementation Method 1

an oil-in-water emulsion base comprising: an emulsifier comprising a mixture of steareth-2 and steareth-20

Methodology Applied
Scientific EffectEmulsion: Emulsion

Implementation Method 2

an emulsifier comprising a mixture of steareth-2 and steareth-20

Methodology Applied
Scientific EffectSurfactant: Surfactant

Implementation Method 3

zinc salts precipitate as hydroxides in the range of pH of 6.5 to 8.0

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 4

increased substantivity of zinc on a skin surface

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentUS11793735B2Aluminum-free antiperspirant / deodorant compositions
Publication Date: 2023.10.24 COLGATE PALMOLIVE CO

AI summary

An aluminum-free antiperspirant/deodorant composition is disclosed. The antiperspirant/deodorant may include an oil-in-water emulsion base and an antiperspirant active dispersed in the oil-in-water emulsion base. The antiperspirant active may be primarily a zinc-based antiperspirant active and the oil-in-water emulsion base may include an emulsifier comprising a mixture of steareth-2 and steareth-20; a plant-based oil, a polyol, and water.