Nickel-Free Zirconium Bulk Amorphous Alloy Design

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Solution Overview

Problem

Amorphous zirconium alloys without nickel and beryllium exhibit smaller critical diameters, making them less suitable for producing massive parts, and pose skin contact and toxicity concerns due to the allergenic potential of nickel and toxicity of beryllium, which are essential for stabilizing the amorphous phase and enhancing corrosion resistance.

Innovation Solution

Development of nickel-free and beryllium-free solid amorphous alloys based on zirconium or hafnium, with additional elements such as copper, aluminum, and iron to increase the critical diameter while maintaining a high ΔTx value, and incorporating specific compositions like Zr-Cu-Fe-Al with additional elements like Ti, Nb, and Ag to achieve a critical diameter greater than 9 mm and excellent corrosion resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If nickel and beryllium are removed from zirconium-based amorphous alloys, then skin contact safety and toxicity are improved, but critical diameter decreases

Engineering Contradiction:
Improveskin contact safetyVSAvoidcritical diameter
Core Design Contradiction:
Object-affected harmful factorsVSLength of stationary object

Solution Approach 1:

The patent changes the chemical composition parameters by removing nickel and beryllium while introducing alternative elements (titanium: 1-5 at.%, niobium: 1-5 at.%, silver: 2-8 at.%, palladium: 1-3 at.%) to maintain the amorphous phase stability and increase critical diameter despite the removal of toxic elements

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite alloy system Zr-Cu-Al-X-Y where X and Y represent multiple additive elements (Ti, Nb, Ag, Pd) that work synergistically to compensate for the removal of nickel and beryllium, achieving both safety and structural integrity

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If nickel and beryllium are removed from zirconium-based amorphous alloys, then skin contact safety is improved, but corrosion resistance deteriorates

Engineering Contradiction:
Improveskin contact safetyVSAvoidcorrosion resistance
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent adjusts compositional parameters by introducing corrosion-resistant elements (palladium: 1-3 at.%, silver: 2-8 at.%) that form protective surface films, compensating for the loss of nickel's corrosion resistance while maintaining skin contact safety

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the potential harm of removing protective elements (nickel's corrosion resistance) into a benefit by introducing alternative elements that provide enhanced corrosion resistance through different mechanisms (palladium's noble metal properties, silver's oxide film formation)

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Object-affected harmful factors

If nickel and beryllium are removed from zirconium-based amorphous alloys, then toxicity is reduced, but glass-forming ability deteriorates

Engineering Contradiction:
ImprovetoxicityVSAvoidglass-forming ability
Core Design Contradiction:
Object-affected harmful factorsVSEase of manufacture

Solution Approach 1:

The patent modifies the compositional parameters by introducing elements with high atomic size difference and negative heat of mixing (niobium: 1-5 at.%, titanium: 1-5 at.%) that enhance glass-forming ability through increased structural complexity and reduced atomic mobility during solidification

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent develops a multi-element composite system Zr-Cu-Al-Ti-Nb-Ag-Pd that leverages the synergistic effects of different elements to achieve superior glass-forming ability, where each element contributes specific properties that collectively enable bulk amorphous formation without toxic constituents

Inventive Principle:
Principle #40Composite materials

Data Source

PatentEP3128035B1Bulk amorphous alloy made of nickel-free zirconium
Publication Date: 2020.03.04 THE SWATCH GRP RES & DEVELONMENT LTD
  • EP3128035B1 patent drawingFigure 1~2

AI summary

A massive, nickel-free, amorphous alloy consisting, in atomic percentages, of: - a zirconium and/or hafnium base, constituting the balance, with a total zirconium and hafnium greater than or equal to 52.0 and less than or equal to 62.0; - copper: greater than or equal to 16.0 and less than or equal to 28.0; - iron: greater than or equal to 0.5 and less than or equal to 10.0; - aluminium: greater than or equal to 7.0 and less than or equal to 13.0; - at least two filler metals (X) taken from the family including Ti, V, Nb, Y, Cr, Mo, Co, Sn, Zn, P, Pd, Ag, Au, Pt, Ta, Ru, Rh, Ir, Os, and Hf when said base does not include any, and Zr when said base does not include any, the cumulative atomic percentage of said filler metals being greater than or equal to 6.0, and less than or equal to 10.0.