Zn-Based Coating With Diffusion Barrier for Hot Forming

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current Zn-based coatings for steel substrates face challenges in high temperature processes and environments due to zinc diffusion, evaporation, micro-crack formation, liquid metal embrittlement, and oxidation, limiting their effectiveness in hot forming operations and high-temperature applications.

Innovation Solution

A Zn-based coating with elevated melting temperatures, such as Zn-Sr, Zn-Ca, or Zn-Mn coatings with specific content ranges, combined with a diffusion barrier layer like tungsten or conductive oxides, and an evaporation/oxidation barrier layer, to prevent zinc diffusion and evaporation while maintaining cathodic corrosion protection.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If Zn-based coatings are used for corrosion protection, then cathodic corrosion protection is provided, but zinc diffusion into the substrate occurs at high temperatures

Engineering Contradiction:
Improvecorrosion protectionVSAvoidzinc diffusion
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

A diffusion barrier layer comprising at least one of tungsten, tantalum, niobium, hafnium, or their oxides is introduced between the steel substrate and the Zn-based coating. This intermediary layer prevents zinc diffusion into the substrate while allowing the Zn-based coating to maintain its cathodic corrosion protection function, thus resolving the contradiction between corrosion protection and zinc loss.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If high temperature hot forming operations are performed, then forming operations can be carried out, but zinc evaporation occurs reducing coating weight

Engineering Contradiction:
Improvehot forming capabilityVSAvoidzinc evaporation
Core Design Contradiction:
ProductivityVSLoss of substance

Solution Approach 1:

The diffusion barrier layer also acts as an evaporation barrier, preventing zinc from evaporating during high temperature hot forming operations. This allows the coating to withstand the high temperatures required for hot forming while maintaining sufficient zinc weight for corrosion protection.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If high temperature processes are applied, then hot forming operations are enabled, but micro-crack formation due to solid metal induced embrittlement occurs

Engineering Contradiction:
Improvehot forming capabilityVSAvoidembrittlement resistance
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The diffusion barrier layer prevents direct contact between the Zn-based coating and the steel substrate at high temperatures, eliminating the mechanism that causes solid metal induced embrittlement. This allows hot forming operations to proceed without micro-crack formation, maintaining the strength and integrity of the steel blank.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Reliability

If Zn-based coatings are used, then cathodic corrosion protection is provided, but liquid metal embrittlement can occur during hot pressing

Engineering Contradiction:
Improvecorrosion protectionVSAvoidembrittlement resistance
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The diffusion barrier layer prevents liquid Zn-phases from penetrating between steel substrate grain boundaries during hot pressing operations. This intermediary barrier eliminates the risk of liquid metal embrittlement while preserving the cathodic corrosion protection provided by the Zn-based coating.

Inventive Principle:
Principle #24Intermediary (Mediator)

5Productivity

If high temperature operations are performed, then hot forming is enabled, but oxidation of the Zn-based coating occurs

Engineering Contradiction:
Improvehot forming capabilityVSAvoidoxidation
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The diffusion barrier layer acts as a protective barrier that prevents oxidation of the Zn-based coating during high temperature hot forming operations. This intermediary layer allows the coating to withstand high temperatures without forming thick oxide layers that would compromise corrosion protection.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables Zn-based coatings to withstand high temperatures, reduce micro-crack and liquid metal embrittlement risks, and maintain effective corrosion protection, making them suitable for hot forming and high-temperature applications without significant zinc loss or oxidation.

Implementation Method 1

a diffusion barrier layer between the substrate and the Zn-based coating, wherein the diffusion barrier layer prevents diffusion of zinc from the Zn-based coating into the substrate

Methodology Applied
Scientific EffectDiffusion barrier: Diffusion Barrier

Implementation Method 2

the Zn-based coating has a melting temperature above 600°C... reduce evaporation of the Zn-based coating

Methodology Applied
Scientific EffectEvaporation resistance: Evaporation

Implementation Method 3

not a cathodic corrosion protection such as provided by Zn-based coatings

Methodology Applied
Scientific EffectCathodic protection:

Data Source

PatentEP3084032B1Steel substrate provided with corrosion resistant coating with high melting temperature and manufacturing method thereof
Publication Date: 2017.09.06 TATA STEEL NEDERLAND TECH BV

AI summary

The invention relates to a steel substrate provided with a Zn-based corrosion resistant coating, wherein the Zn-based coating has a melting temperature above 600°C which makes it suitable for forming operations at elevated temperatures.