Method for producing heterometal hydrogenation catalysts

By employing a controlled reduction process with a specific reducing gas, the method addresses catalyst deactivation and performance issues, achieving efficient conversion of dicarboxylic acids to dialcohols and high yield of cyclohexanedimethanol.

JP7873672B2Active Publication Date: 2026-06-12HANWHA SOLUTIONS CORP
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Patent Information

Application Number
JP2023544684
Authority / Receiving Office
JP · JP
Patent Type
Patents
Current Assignee / Owner
Priority Date
2021-02-01
Filing Date
2022-01-19
Publication Date
2026-06-12
Estimated Expiration
2042-01-19

AI Technical Summary

Technical Problem

Existing methods for manufacturing heterogeneous metal hydrogenation catalysts face challenges such as respiratory toxicity, environmental pollution, and inefficient reduction conditions, leading to catalyst deactivation and performance issues, especially in dissimilar metal catalysts.

Method used

A method involving the use of a specific reducing gas under controlled temperature and gas supply conditions to reduce heterometal catalysts, ensuring uniform alloy formation and preventing segregation or sintering, using a reactor with supported heterometal compounds.

Benefits of technology

This approach allows for the production of a catalyst with uniform active metal distribution, enhancing catalytic activity and efficiency in converting dicarboxylic acid groups to dialcohol groups, with a yield of cyclohexanedimethanol exceeding 70%.

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Abstract

The present invention relates to a method for producing a heterogeneous metal hydrogenation catalyst, and more specifically, is characterized in that the hydrogenation reaction of the catalyst is improved when the hydrogenation catalyst is reduced under appropriate reduction conditions using a specific reducing gas.
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