AFM Tip Characterization Structure Using Diamond-Like Carbon

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Solution Overview

Problem

Existing characterization structures for atomic force microscope tips suffer from erosion issues when trying to determine the shape and dimensions of complex tips, leading to inaccurate and unreliable measurements due to the thinning of tips, which results in radii of curvature greater than the tips being characterized, preventing sufficient measurement points from being acquired.

Innovation Solution

A characterization structure with a first support element and a first characterization element of constant thickness, where the characterization surfaces are not fine and remain constant or reduce uniformly, allowing for accurate characterization of flared, cylindrical, and conical tips without the need for thinning, and utilizing amorphous diamond-like carbon and electron beam-assisted localized growth for manufacturing.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If characterization structures with fine tips are used to determine the shape of AFM tips, then measurement precision is improved, but the tips erode and radii of curvature increase, reducing reliability

Engineering Contradiction:
Improvetip shape characterization accuracyVSAvoidmeasurement reliability
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent creates a calibration structure that is a simplified copy of the tip geometry (a ridge with parallel sides representing the tip width) rather than using an actual fine tip. This copy structure has constant dimensions and does not erode, providing reliable reference data for tip characterization without suffering from tip erosion problems.

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The calibration structure is designed as a robust, easily replaceable component with constant geometry that does not require maintenance. Unlike eroding fine tips that need frequent replacement, this structure provides long-term stable reference measurements.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Measurement precision

If fine tips are used for characterization, then measurement precision is improved, but service life is reduced due to erosion

Engineering Contradiction:
Improvetip shape measurement accuracyVSAvoidcharacterization structure service life
Core Design Contradiction:
Measurement precisionVSDuration of action of moving object

Solution Approach 1:

Instead of using actual fine tips that erode, the patent employs a calibration structure that copies the essential geometric features (width, position) in a robust form factor. This structure maintains constant dimensions over time, providing enduring reference points for tip characterization without the erosion that limits fine tip service life.

Inventive Principle:
Principle #26Copying

3Measurement precision

If conventional VPS structures are used for diameter measurement, then overall diameter can be determined, but shape characterization is insufficient

Engineering Contradiction:
Improveoverall diameter measurementVSAvoidtip shape characterization capability
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent merges the diameter measurement function and shape characterization function into a single integrated calibration structure. The ridge structure provides both the width reference for overall diameter determination and the positional references for shape characterization, eliminating the need for separate VPS and shape characterization structures.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The calibration structure serves multiple functions: it provides reference points for overall diameter measurement, shape characterization, and tip wear monitoring. This universal structure replaces multiple specialized structures, providing versatile characterization capability for various tip types including flared, cylindrical, and conical shapes.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The structure ensures optimal characterization of AFM tips with a long service life, maintaining accuracy and reproducibility even when tips become eroded, and can characterize any type of tip, including flared, cylindrical, and conical shapes, providing stable and consistent data.

Implementation Method 1

utilizing amorphous diamond-like carbon and electron beam-assisted localized growth for manufacturing

Methodology Applied
Scientific EffectElectron beam-assisted localized growth: Electron Beam

Data Source

PatentEP2657711B1Characterization structure for an atomic force microscope tip
Publication Date: 2019.08.07 NANOTOOLS
  • EP2657711B1 patent drawingFigure 1~2d
  • EP2657711B1 patent drawingFigure 3a~4
  • EP2657711B1 patent drawingFigure 5a~6b

AI summary

The invention concerns a structure (40) for the characterization of a tip of an atomic force microscope. The structure (40) is produced on a substrate (41) and comprises: ● a first support element (42) located above the substrate (41); ● a first characterization element (45) with a constant thickness (e1), said first characterization element (45) being located above said first support element (42) and having an upper flat surface (46) and a lower flat surface (47) covering the upper surface of said first support element (42) with at least one zone (P1, P2) extending beyond said upper surface of said first support element (42), said zone (P1, P2) having a characterization surface (48, 49) at one end which is capable of coming into contact with a tip to be characterized, the upper surface (46) and the lower surface (47) of said first characterization element (45) being parallel to the upper surface (52) of said substrate (41).