Air-Cooled ICP-MS Interface to Limit Ion Recombination

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Solution Overview

Problem

Conventional inductively coupled plasma mass spectrometers (ICP-MS) rely on water-cooling systems, which are costly, complex, and bulky, and result in ion recombination and clustering due to reduced ion beam temperature, limiting sensitivity and increasing system size and cost.

Innovation Solution

An air-cooled interface for ICP-MS systems using fins, open-cell metal foams, compact heat exchangers, or heat pipes to manage heat dissipation, with adjustable thermal resistors to direct heat away from sensitive components and prevent recombination, utilizing natural or forced convection to enhance cooling efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If water-cooling systems are used to cool the sampling interface, then heat dissipation is effective, but system size, cost, and complexity increase significantly

Engineering Contradiction:
Improvecooling efficiencyVSAvoidsystem complexity
Core Design Contradiction:
TemperatureVSDevice complexity

Solution Approach 1:

The invention extracts the cooling function from the complex water-cooling system with chillers and coolant circulation, and implements it directly through air cooling of the sampling interface components. This eliminates the need for separate cooling systems while maintaining effective heat dissipation.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention introduces air as an intermediary cooling medium between the hot sampling interface and the environment. By using air cooling with heat sinks and fins, the system achieves effective heat transfer without requiring water circulation systems, chillers, or complex coolant management infrastructure.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Temperature

If water-cooling systems are used to cool the sampling interface, then heat dissipation is effective, but system size and weight increase

Engineering Contradiction:
Improvecooling efficiencyVSAvoidsystem weight
Core Design Contradiction:
TemperatureVSWeight of stationary object

Solution Approach 1:

The invention removes the heavy chiller units and coolant storage systems from the ICP-MS setup by implementing direct air cooling. The sampling interface components themselves serve as heat sinks, eliminating the need for separate cooling equipment that would add significant weight.

Inventive Principle:
Principle #2Taking out (Extraction)

3Temperature

If water-cooling systems are used to cool the sampling interface, then heat dissipation is effective, but cost increases due to equipment and maintenance

Engineering Contradiction:
Improvecooling efficiencyVSAvoidsystem cost
Core Design Contradiction:
TemperatureVSEase of manufacture

Solution Approach 1:

The invention eliminates expensive chiller equipment, coolant circulation pumps, and associated infrastructure by using simple air cooling. This dramatically reduces both the initial equipment cost and ongoing maintenance costs related to coolant management and system complexity.

Inventive Principle:
Principle #2Taking out (Extraction)

4Temperature

If water-cooling systems are used to cool the sampling interface, then heat dissipation is effective, but ion recombination and clustering occur due to reduced ion beam temperature

Engineering Contradiction:
Improvecooling efficiencyVSAvoidsensitivity
Core Design Contradiction:
TemperatureVSMeasurement precision

Solution Approach 1:

The invention applies local quality by differentiating the thermal treatment of different components. The sampling interface components (sampler cone, skimmer cone) are air-cooled to prevent heat damage, while the ion beam path is maintained at higher temperatures through thermal isolation. This selective thermal management prevents ion recombination in the beam path while effectively cooling the interface components.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention uses air as a cooling intermediary that does not contact the ion beam, unlike water cooling which directly cools the interface components through which ions pass. This indirect air cooling approach prevents heat transfer to the ion beam, avoiding ion recombination and clustering while still achieving effective heat dissipation from the interface components.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The air-cooled interface reduces system size, cost, and complexity while improving cooling efficiency, preventing heat transfer to sensitive components and minimizing ion recombination, thereby enhancing sensitivity and reducing detection limits.

Implementation Method 1

utilizing natural or forced convection to enhance cooling efficiency

Methodology Applied
Scientific EffectConvection: Convection

Implementation Method 2

An air-cooled interface for ICP-MS systems using fins, open-cell metal foams, compact heat exchangers, or heat pipes to manage heat dissipation

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Implementation Method 3

with adjustable thermal resistors to direct heat away from sensitive components and prevent recombination

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentUS11864303B2Air-cooled interface for inductively coupled plasma mass spectrometer (ICP-MS)
Publication Date: 2024.01.02 KIMIA ANALYTICS INC
  • US11864303B2 patent drawing
  • US11864303B2 patent drawing
  • US11864303B2 patent drawing

AI summary

An air cooled inductively coupled plasma mass spectrometer (ICP-MS) is disclosed. The interface structure has a configuration that it can rapidly transfer heat away from the front surface of the interface that is exposed to a high temperature plasma, while maintaining heat in the ion beam to avoid recombination and clustering. The air cooled interface of the present system comprises of a set of fins for rapid heat transfer, which may be placed along the sides of the ICP-MS systems in a variety of orientations. Open-cell metal foam is also used to increase heat transfer efficiency. The system may be cooled by natural convention or forced convection using one or more air fans.