Alloy-Composite Negative Electrode for Li-Ion Batteries

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Solution Overview

Problem

Graphite-based negative electrode active materials in lithium-ion batteries face challenges with capacity deterioration due to significant volume expansion and contraction, leading to cracking and loss of electron conductivity, which limits their cycle life and capacity retention.

Innovation Solution

A negative electrode active material comprising a carbonaceous powder material with a specific Raman spectrum peak intensity ratio and an alloy phase that undergoes thermoelastic diffusionless transformation, mitigating strain and improving discharge capacity and cycle characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If alloy-based negative electrode active materials (Si or Sn) are used to achieve higher capacity, then discharge capacity per mass is improved, but volume expansion/contraction during charging/discharging causes cracking and capacity deterioration

Engineering Contradiction:
Improvedischarge capacity per massVSAvoidcharge-discharge cycle characteristics
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention uses a composite material system consisting of alloy particles (Si or Sn) combined with a specific binder material. The binder material forms a matrix that encapsulates the alloy particles, creating a composite structure that maintains the high capacity benefits of the alloy while mitigating the volume expansion/contraction problem through the binder's mechanical properties and volume change compensation capability.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention changes the physical and chemical parameters of the negative electrode by introducing a binder material with specific properties (carbonaceous material with controlled graphitization degree, specific Raman spectrum characteristics). This parameter change transforms the electrode structure from pure alloy particles to a composite system where the binder's volume change characteristics compensate for the alloy's expansion/contraction, improving cycle stability.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If graphite-based negative electrode active materials are used, then volume stability is maintained, but discharge capacity per mass is limited

Engineering Contradiction:
Improvevolume stabilityVSAvoiddischarge capacity per mass
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The invention creates a composite negative electrode active material that combines alloy particles (providing high capacity) with binder material (providing volume stability). This composite structure allows the electrode to achieve discharge capacity per mass exceeding that of conventional graphite while maintaining volume stability through the binder's mechanical support and volume change compensation.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention applies different material properties to different components of the negative electrode: alloy particles provide high capacity in specific regions, while the binder material provides volume stability and structural support in the matrix. This local differentiation of material qualities allows the overall electrode to achieve both high capacity and volume stability simultaneously.

Inventive Principle:
Principle #3Local quality

3Quantity of substance

If Si or Sn single substance is used, then discharge capacity per mass is significantly improved, but volume expansion/contraction ratio reaches about 400% causing cracking

Engineering Contradiction:
Improvedischarge capacity per massVSAvoidvolume expansion/contraction
Core Design Contradiction:
Quantity of substanceVSShape

Solution Approach 1:

The invention forms a composite where alloy particles (Si or Sn) are embedded in a binder material matrix. The binder material's volume change characteristics are specifically selected to compensate for the 400% volume expansion/contraction of the alloy particles, maintaining overall electrode shape stability while preserving the high capacity benefits of the alloy.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The binder material acts as an intermediary between the alloy particles and the electrode structure. It mediates the volume expansion/contraction by providing a compliant matrix that absorbs and distributes the mechanical stress, preventing direct cracking of the alloy particles and maintaining electrical connectivity throughout charge-discharge cycles.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed material enhances discharge capacity per mass, cycle life, and reduces irreversible capacity by relaxing strain through thermoelastic diffusionless transformation, resulting in improved performance compared to conventional alloy-based and graphite-based materials.

Implementation Method 1

Material C: powder material whose main component is an active substance made up of an alloy phase. This alloy phase undergoes thermoelastic diffusionless transformation when releasing metal ions or occluding the metal ions.

Methodology Applied
Scientific EffectThermoelastic diffusionless transformation: Phase Change

Implementation Method 2

the negative electrode material of Patent Literature 1 includes a Ti-Ni superelastic alloy, and Si particles formed in the superelastic alloy

Methodology Applied
Scientific EffectElectron conduction: Conduction (electrical)

Data Source

PatentEP3113258B1Negative electrode active substance material, negative electrode, and cell
Publication Date: 2019.04.03 NIPPON STEEL CORPORATION
  • EP3113258B1 patent drawingFigure 1
  • EP3113258B1 patent drawingFigure 2A~2B
  • EP3113258B1 patent drawingFigure 2C~2E

AI summary

Provided is a negative electrode active material which can improve discharge capacity per amount and charge-discharge cycle characteristics. The negative electrode active material of the present embodiment contains at least one of material A and material B, and material C: Material A: carbonaceous powder material in which a ratio of a peak intensity at 1360 cm-1 with respect to a peak intensity at 1580 cm-1 in the Raman spectrum is not more than 0.5; Material B: carbonaceous powder material in which a ratio of a peak intensity at 1360 cm-1 with respect to a peak intensity at 1580 cm-1 in the Raman spectrum is more than 0.5; Material C: powder material whose main component is an active substance made up of an alloy phase. This alloy phase undergoes thermoelastic diffusionless transformation when releasing metal ions or occluding the metal ions.