Aqueous Material Phase-Change Extrusion for Continuous Freezing

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Solution Overview

Problem

Existing batch freezing methods for liquid aqueous materials, such as milk and juice, result in preferential freezing, solute concentration, and mechanical damage, leading to product degradation and increased handling costs, especially in small-scale facilities with infrequent transportation.

Innovation Solution

A continuous process and apparatus that rapidly freezes liquid aqueous materials within a tube under pressure, forming a self-lubricating frozen extrusion with dendritic crystals, allowing for continuous production of discrete frozen units.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If batch freezing is used to freeze liquid aqueous material, then the material can be stored in frozen form, but the process is slow and causes preferential freezing of pure water, creating reduction in freezing point of remaining aqueous component and concentration of other solutes

Engineering Contradiction:
Improveproduct integrityVSAvoidfreezing speed
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent changes the freezing rate parameter from slow (batch) to rapid (continuous), which fundamentally alters the freezing behavior. Rapid freezing prevents preferential freezing of pure water and avoids solute concentration, while maintaining product integrity through controlled phase change dynamics

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention implements continuous freezing through a continuous process where liquid aqueous material is continuously fed into a freezing extrusion device and continuously frozen as it passes through the device, eliminating the intermittent nature of batch processing and maintaining consistent product quality

Inventive Principle:
Principle #20Continuity of useful action

2Reliability

If slow freezing occurs in batch process, then the material can be frozen, but gross segregation of components occurs causing mechanical damage to food components and structures

Engineering Contradiction:
Improveproduct integrityVSAvoidprocess simplicity
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

By changing the freezing rate from slow to rapid, the patent prevents gross segregation of components. The rapid freezing creates a fine crystal structure that embeds food components within the ice matrix, preventing mechanical damage while maintaining product integrity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the mechanical mixing and handling operations required in batch processing with a continuous fluid-based freezing process. The continuous feeding and freezing mechanism eliminates the need for extensive product handling, reducing mechanical damage risks

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Reliability

If batch freezing is used, then the material can be frozen, but extensive product handling is required to fill vessels, empty them, and repack frozen products increasing labor and capital costs

Engineering Contradiction:
Improvestorage capabilityVSAvoidhandling requirements
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The continuous freezing process eliminates the need for filling, emptying, and repacking operations. Material is continuously fed into the freezing device and continuously produced as frozen extrusion, which can be directly packaged or stored without intermediate handling steps

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system produces frozen material in a continuous form that is ready for direct use or storage. The continuous extrusion format eliminates the need for complex vessel handling and repacking operations, allowing the system to serve its own storage and packaging needs

Inventive Principle:
Principle #25Self-service

4Reliability

If rapid freezing is used to prevent solute concentration and mechanical damage, then product integrity is maintained, but the process requires continuous operation and specialized equipment

Engineering Contradiction:
Improveproduct integrityVSAvoidequipment requirements
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The freezing extrusion device performs multiple functions: it freezes the material, forms the frozen extrusion shape, and enables continuous processing. This multi-functionality reduces the need for separate specialized equipment while maintaining rapid freezing capabilities and product integrity

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process maintains product integrity by preventing mechanical damage and solute concentration, reducing handling costs, and enabling efficient storage and transportation of frozen materials in discrete units.

Implementation Method 1

cooling the liquid aqueous material to cause a progressive phase change in which substantially all of the aqueous material changes from liquid form to frozen form within the tube

Methodology Applied
Scientific EffectHeat transfer: Conduction (thermal)

Implementation Method 2

cooling the liquid aqueous material to cause a progressive phase change in which substantially all of the aqueous material changes from liquid form to frozen form within the tube

Methodology Applied
Scientific EffectPhase change: Phase Change

Implementation Method 3

continuously pumping aqueous material in liquid form into the tube inlet under pressure

Methodology Applied
Scientific EffectPressure: Pressure Increase

Implementation Method 4

pumping the aqueous material through the tube from the tube inlet to the tube outlet

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Data Source

PatentUS12414575B2Process and apparatus for phase-change extrusion of aqueous material
Publication Date: 2025.09.16 MASSEY UNIVERSITY
  • US12414575B2 patent drawing
  • US12414575B2 patent drawing
  • US12414575B2 patent drawing

AI summary

The invention relates to a continuous process for freezing a flow of aqueous material in liquid form and moving the aqueous material through at least one tube from an inlet of the tube to an outlet of the tube so as to form a breakable or cuttable frozen extrusion without bursting the tube. The process creates an extruded material that comprises liquid aqueous material entrapped between frozen aqueous material to self-lubricate the extrusion as it moves through the tube. An apparatus for carrying out the process of the invention is also provided.