HCFO-1233yd(Z)-tDCE Azeotropic Composition for Stable Cycling

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Solution Overview

Problem

Existing compositions using fluoroolefins in combination with other components face issues of composition change due to boiling point differences and safety concerns, particularly when evaporated and condensed repeatedly, affecting performance and safety.

Innovation Solution

The development of azeotropic and azeotrope-like compositions comprising (Z)-1-chloro-2,3,3-trifluoropropene (HCFO-1233yd(Z)) and trans-1,2-dichloroethylene (tDCE) with specific mass ratios, ensuring stability and non-flammability, and allowing for repeated evaporation and condensation without significant composition change.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If fluoroolefins are used in combination with other components, then required performance can be sufficiently developed, but composition change occurs during use due to boiling point differences

Engineering Contradiction:
ImproveperformanceVSAvoidcomposition stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent forms an azeotropic composition by selecting specific components (fluoroolefin and hydrocarbon) in predetermined proportions that create a constant boiling point mixture. This parameter change from individual component properties to mixture properties resolves the composition instability issue while maintaining the enhanced performance benefits of combination use.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite azeotropic mixture of fluoroolefin and hydrocarbon components with specific mass ratios. This composite material approach allows the system to achieve the performance advantages of multi-component combinations while eliminating the composition separation problem through the azeotropic effect.

Inventive Principle:
Principle #40Composite materials

2Reliability

If components with flash point are used in combination, then performance requirements can be met, but safety countermeasures are required

Engineering Contradiction:
ImproveperformanceVSAvoidflammability
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent uses hydrocarbon components that create a non-flammable or low-flammability environment when mixed with fluoroolefin in azeotropic proportions. This inert environment approach eliminates the need for safety countermeasures while maintaining the performance benefits of component combination.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

3Stability of the object's composition

If CFCs, HCFCs and HFCs are used, then stability and drying property are excellent, but they have negative influences over the ozone layer and global warming

Engineering Contradiction:
ImprovestabilityVSAvoidenvironmental impact
Core Design Contradiction:
Stability of the object's compositionVSObject-generated harmful factors

Solution Approach 1:

The patent changes the chemical composition parameters from traditional CFC/HCFC/HFC compounds to fluoroolefin-hydrocarbon azeotropic mixtures. This parameter change maintains the desirable stability and drying properties while eliminating the harmful environmental effects of ozone depletion and global warming.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the potential harm of using alternative refrigerants into a benefit by selecting fluoroolefin-hydrocarbon combinations that provide both environmental friendliness and operational stability. The azeotropic composition ensures that the alternative refrigerant mixture performs as reliably as traditional refrigerants without the environmental damage.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The compositions exhibit stable performance as detergents, solvents, and heat transfer fluids with minimal environmental impact, maintaining consistency across multiple cycles and avoiding flammability, suitable for various applications including cleaning and heat transfer systems.

Implementation Method 1

an azeotropic composition, an azeotrope-like composition and a composition, which have little influence over the global environment, which are non-flammable, and which are less likely to undergo composition change even when evaporated and condensed repeatedly

Methodology Applied
Scientific EffectAzeotropic effect:

Data Source

PatentEP3981756B1Azeotropic composition, azeotrope-like composition, composition, cleaning agent, solvent, and heat transfer medium
Publication Date: 2025.07.02 AGC INC
  • EP3981756B1 patent drawingFigure 1

AI summary

To provide an azeotropic composition, an azeotrope-like composition and a composition, which have little influence over the global environment, which are non-flammable, and which are less likely to undergo composition change even when evaporated and condensed repeatedly, and a detergent, a solvent and a heat transfer fluid, which contain the azeotropic composition, the azeotrope-like composition or the composition. An azeotropic composition consisting essentially of 34.5 mass% of (Z)-1-chloro-2,3,3-trifluoropropene and 65.5 mass% of trans-1,2-dichloroethylene, and an azeotrope-like composition consisting essentially of from 28 to 41 mass% of (Z)-1-chloro-2,3,3-trifluoropropene and from 59 to 72 mass% of trans-1,2-dichloroethylene.