Backscattering Sensor for Crystallization Degree Detection

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Solution Overview

Problem

Current methods for detecting the degree of crystallization and disperse surface in mediums, especially for non-spherical particles and high concentrations, are inefficient and costly, lacking direct measurement capabilities and requiring complex setups, which hinders process optimization in industries like sugar production.

Innovation Solution

A measuring device emitting primary radiation into the medium to generate secondary radiation, with a spatially limited radiation area and a radiation receiver to detect backscattering, allowing for the quantification of disperse surface changes over time, enabling inline monitoring and process control.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If direct light scattering (DLS) measurements are used for particle size analysis, then the setup is simple, but it becomes inapplicable for large particles and non-spherical particles due to anisotropic scattering

Engineering Contradiction:
Improvemeasurement setup complexityVSAvoidapplicability to different particle types
Core Design Contradiction:
Device complexityVSAdaptability or versatility

Solution Approach 1:

The patent changes the measurement parameter from angular-dependent scattering patterns (anisotropic) to total backscattering intensity (isotropic). By integrating the scattering signal over all angles and using a spherically symmetric detection geometry, the measurement becomes independent of particle shape and orientation, enabling universal application to all particle types while maintaining setup simplicity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces complex mechanical particle analysis systems (such as image analysis or sequential angular scanning) with an optical backscattering measurement system. The key substitution is replacing the need for complex particle-by-particle mechanical or visual inspection with a bulk optical measurement that directly yields dispersed surface area through light scattering intensity

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Measurement precision

If conventional sensors are used to measure dispersed surface area, then measurement is possible, but the sensors are considerably more expensive and complex

Engineering Contradiction:
Improvedispersed surface area measurement capabilityVSAvoidsensor complexity and cost
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts only the essential measurement information (total backscattering intensity) needed to determine dispersed surface area, eliminating the need for complex particle size distribution analysis, shape factor calculations, or multiple measurement angles. This extraction of the core measurable quantity simplifies the sensor design while maintaining measurement precision for the specific parameter of dispersed surface area

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent creates a universal measurement principle based on the fundamental relationship between backscattering intensity and dispersed surface area that applies to all particle types, concentrations, and sizes. This universal approach replaces multiple specialized sensors with a single versatile backscattering sensor that can measure dispersed surface area across diverse applications

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Productivity

If crystal concentration is increased to improve yield, then production efficiency increases, but anisotropic scattering behavior makes surface area quantification more difficult

Engineering Contradiction:
Improvecrystallization yield and throughputVSAvoiddispersed surface area quantification
Core Design Contradiction:
ProductivityVSDifficulty of detecting and measuring

Solution Approach 1:

The patent employs continuous dynamic measurement of backscattering intensity as crystals grow and change concentration in the medium. The real-time monitoring capability allows the system to track dispersed surface area changes during crystallization processes, providing continuous feedback for process optimization despite varying crystal concentrations and anisotropic scattering behaviors

Inventive Principle:
Principle #18Mechanical vibration

Solution Approach 2:

The patent transforms the measurement approach by changing from particle-specific parameters (individual size and shape) to a bulk parameter (total backscattering intensity proportional to dispersed surface area). This parameter transformation enables accurate measurement even at high crystal concentrations where individual particle characteristics become difficult to resolve

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution provides a cost-effective and efficient means to monitor crystallization processes, offering real-time feedback for dynamic process adjustments, ensuring consistent product quality and minimizing failure rates by quantifying disperse surface changes, thereby improving process efficiency.

Implementation Method 1

due to their anisotropic scattering

Methodology Applied
Scientific EffectLight scattering: Scattering

Implementation Method 2

the backscattering behavior

Methodology Applied
Scientific EffectBackscattering: Reflection

Data Source

PatentEP4058785B1Sensor and device for detecting the degree of crystallization
Publication Date: 2025.01.01 SUDZUCKER AG MANNHEIM OCHSENFURT
  • EP4058785B1 patent drawingFigure 1
  • EP4058785B1 patent drawingFigure 2a~3
  • EP4058785B1 patent drawingFigure 4

AI summary

A measurement apparatus is proposed for detecting the degree of crystallization of a medium and/or for detecting the disperse surface in the medium, the measurement apparatus comprising a radiation source for emitting primary radiation into the medium, in particular a light source, wherein the primary radiation is transmitted in a primary beam direction and emerges from the radiation source, wherein the radiation source is configured to radiate the primary radiation into the medium in such a way that a spatially restricted measurement volume is provided in order to generate secondary radiation in the measurement volume, and a radiation receiver for receiving at least some of the secondary radiation generated in the measurement volume, wherein the radiation receiver is located outside the primary beam direction and wherein the radiation receiver is configured to receive and transmit the secondary radiation and/or to output an output signal.