Biobased Block Copolymer Composition for Extensible Degradable PHAs

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing block copolymers synthesized from petroleum-based resources lack diversity in structural units and do not fully leverage the potential of biopolymers for improved physical properties, such as extensibility and degradability, necessitating the development of biopolymers with varied structural units.

Innovation Solution

Culturing microorganisms in media containing specific combinations of hydroxycarboxylic acids, including 2-hydroxybutyric acid and 3-hydroxyhexanoic acid, with enzymes like CoA transferase and polymerizing enzymes, to biosynthesize block copolymers with homopolymer and copolymer segments, such as P(2HB-b-(3HB-co-3HHx), P(3HB-b-(GL-co-3HB)), and P(3HB-b-(GL-co-3HHx)) to enhance extensibility and degradability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If block copolymers are synthesized using conventional petroleum-based methods, then production efficiency is maintained, but material diversity and environmental sustainability are limited

Engineering Contradiction:
Improvematerial diversityVSAvoidproduction complexity
Core Design Contradiction:
Adaptability or versatilityVSEase of manufacture

Solution Approach 1:

The invention changes the fundamental parameter of raw material source from petroleum-based to biomass-based (renewable resources). This parameter change enables material diversity through different biomass feedstocks while maintaining production feasibility through established biopolymer synthesis pathways

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates composite block copolymer structures combining segments from different biomass-derived monomers (e.g., polyhydroxyalkanoate segments with other biopolymer segments). This composite approach achieves material diversity by integrating properties of different biopolymers while using renewable resources

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If random copolymers are biosynthesized in microorganisms, then production simplicity is maintained, but structural control and property optimization are limited

Engineering Contradiction:
Improvestructural controlVSAvoidbiosynthesis complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention segments the copolymer structure into distinct blocks with specific compositions and sequences. By controlling the biosynthesis to produce block copolymers rather than random copolymers, the invention achieves precise structural control over polymer properties while managing biosynthesis complexity through targeted metabolic engineering

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention employs preliminary action by pre-designing the metabolic pathways and enzyme systems in microorganisms to produce specific block copolymer structures. This preliminary engineering of the biosynthetic system enables controlled production of desired polymer architectures before actual polymerization occurs

Inventive Principle:
Principle #10Preliminary action

3Strength

If single-type homopolymer segments are used in block copolymers, then synthesis simplicity is maintained, but physical property optimization is limited

Engineering Contradiction:
Improvephysical propertiesVSAvoidcopolymer structure
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The invention creates composite block copolymers integrating segments from different biopolymer types (e.g., P(3HB) blocks with P(4HB) blocks or other PHA variants). This composite structure optimizes physical properties by combining characteristics of different polymers while managing structural complexity through systematic block design

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention applies local quality by assigning different polymer segments with specific properties to different regions of the copolymer chain. Each block is designed with tailored composition and sequence to provide localized functional properties, optimizing overall material performance through spatial differentiation

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting block copolymers exhibit significantly improved extensibility, degradability, and flexibility, with P(2HB-b-(3HB-co-3HHx) showing extensibility over 1200% and P(3HB-b-(GL-co-3HB-co-3HHx) featuring a gradient structure for enhanced flexibility and hydrolyzability.

Implementation Method 1

culturing microorganisms in media containing specific combinations of hydroxycarboxylic acids, including 2-hydroxybutyric acid and 3-hydroxyhexanoic acid, with enzymes like CoA transferase and polymerizing enzymes, to biosynthesize block copolymers

Methodology Applied
Scientific EffectEnzyme catalysis: Enzyme

Data Source

PatentEP4116428B1Block copolymer and method for producing same
Publication Date: 2025.11.12 HOKKAIDO UNIVERSITY
  • EP4116428B1 patent drawingFigure 1A
  • EP4116428B1 patent drawingFigure 1B
  • EP4116428B1 patent drawingFigure 1C

AI summary

A copolymer comprising: a hydroxycarboxylic acid (A) having a hydroxy group only at a 2-position; and a hydroxycarboxylic acid (B) having a hydroxy group at a position other than a 2-position, and having a homopolymer segment composed of one hydroxycarboxylic acid selected from the group consisting of the hydroxycarboxylic acid (A) and the hydroxycarboxylic acid (B), and a copolymer segment containing at least two hydroxycarboxylic acids selected from the group consisting of the hydroxycarboxylic acid (A) and the hydroxycarboxylic acid (B) .