Calcium Phosphate Carrier Stabilizes Vitamin D Against Oxidation

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Solution Overview

Problem

Existing compositions for human and animal nutrition and pharmaceuticals face challenges in stabilizing active compounds like vitamin D, which are prone to oxidation and isomerization, and struggle with homogeneous dispersion and long-term stability.

Innovation Solution

A stable solid composition is developed using a calcium phosphate carrier with low water solubility and a hydrophobic stabilizer, such as C3-22 fatty acids or their ester derivatives, to enhance the stability and dispersion of oil-soluble active components like vitamins and antioxidants.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If active compounds are dissolved or dispersed in liquid solvent and coated on particulate materials, then incorporation in food and bioassimilation are improved, but stability in time deteriorates due to oxidation and isomerization

Engineering Contradiction:
Improveincorporation in foodVSAvoidstability in time
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent changes the physical state parameter from liquid solvent to solid carrier (particulate material), and modifies the chemical environment by selecting specific carriers (silica, calcium carbonate, calcium phosphate) with different surface properties and solubilities. This parameter change transforms the formulation from a liquid-based coating to a solid adsorbate system, improving stability while maintaining ease of incorporation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates composite formulations by combining active compounds with stabilizers (antioxidants, emulsifiers) and carriers (silica, calcium carbonate, calcium phosphate). These composite materials provide synergistic effects where the carrier provides structural support and adsorption, stabilizers prevent oxidation and isomerization, and the combination achieves both ease of incorporation and long-term stability

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If small amounts of active compound are added to composition, then dosage precision is improved, but homogeneous dispersion deteriorates

Engineering Contradiction:
Improvedosage precisionVSAvoidhomogeneous dispersion
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The patent utilizes porous particulate carriers (silica, calcium carbonate, calcium phosphate) that provide high surface area and porous structure for adsorption. These porous materials can effectively adsorb small amounts of active compounds throughout their structure, ensuring homogeneous dispersion even at low concentrations while maintaining precise dosage control

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent introduces stabilizers as intermediary substances between the active compound and the carrier matrix. These stabilizers (antioxidants, emulsifiers) facilitate uniform distribution of the active compound within the composition, preventing aggregation and ensuring homogeneous dispersion while maintaining dosage precision

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If active compounds are stabilized by mixing with stabilizer and coating material, then stability is improved, but complexity of manufacture increases

Engineering Contradiction:
ImprovestabilityVSAvoidcomplexity of manufacture
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent combines multiple functions into a single integrated system: the carrier provides adsorption and structural support, stabilizers provide oxidation protection and emulsification, and the formulation achieves homogeneous dispersion. This merging of functions into a unified particulate composition simplifies the manufacturing process compared to separate coating and stabilization steps

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent simplifies manufacturing by changing the formulation approach from liquid coating to solid-state adsorption. The active compound is directly adsorbed onto the particulate carrier in solid form, eliminating complex coating processes, drying steps, and equipment requirements associated with liquid application methods

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition effectively prevents oxidation and maintains the stability of active components like vitamin D for extended periods, significantly improving their shelf life and bioavailability.

Implementation Method 1

a stable solid composition comprising a first carrier and an adsorbate adsorbed thereon

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

contributes to the enhancement of the stability of the said at least one active component, e.g., by preventing oxidation thereof

Methodology Applied
Scientific EffectOxidation prevention: Oxidation

Data Source

PatentEP2584913B1Stabilized active compound
Publication Date: 2019.03.20 PRAYON SA
  • EP2584913B1 patent drawingFigure 1~3
  • EP2584913B1 patent drawingFigure 4~6

AI summary

The present invention relates to stable solid compositions comprising a first carrier and an adsorbate comprising at least one active component such as a vitamin D derivative and a hydrophobic stabilizer thereof, characterized in that said first carrier is a calcium phosphate or derivatives thereof having a solubility in water lower than 0.1 wt% at room temperature.