Capsular Polysaccharide Production Without pH Adjustment

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing methods for producing capsular polysaccharides of pneumococcal serotypes require pH adjustment for protein precipitation, which complicates the process and can modify the polysaccharides, generating harmful substances.

Innovation Solution

A method involving cultivating bacterial cells without pH adjustment until the culture broth reaches a pH of 5.5 or lower, allowing natural acidification products to facilitate protein precipitation, eliminating the need for a pH adjuster and simplifying the process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If pH adjustment is performed for protein precipitation, then protein removal efficiency is improved, but process complexity increases and capsular polysaccharide modification occurs

Engineering Contradiction:
Improveprotein removal efficiencyVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The culture broth system automatically lowers its own pH through natural acidification by metabolic byproducts (lactic acid, acetic acid) during extended cultivation, eliminating the need for external pH adjusters. The bacteria themselves serve the function of acidifying the medium for protein precipitation.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The harmful metabolic byproducts (organic acids) that accumulate during cultivation and lower pH are converted into a beneficial tool for protein precipitation. The naturally produced acidification, originally a waste product, becomes the mechanism for simplifying the purification process.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Manufacturing precision

If pH adjuster is used for protein precipitation, then protein precipitation is achieved, but harmful substances are generated

Engineering Contradiction:
Improveprotein precipitationVSAvoidharmful substance generation
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The system uses its own metabolic byproducts (lactic acid, acetic acid) to achieve protein precipitation, eliminating the need for external chemical pH adjusters that would introduce harmful substances into the capsular polysaccharide product.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

Metabolic byproducts that were previously considered waste or harmful are converted into the precipitating agent, eliminating the introduction of external harmful chemicals while achieving the same protein precipitation effect.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Ease of manufacture

If additional cultivating is performed without pH adjustment, then pH reaches 5.5 or lower naturally, but cultivation time increases

Engineering Contradiction:
Improveprocess simplificationVSAvoidcultivation time
Core Design Contradiction:
Ease of manufactureVSLoss of time

Solution Approach 1:

The cultivation process continues uninterrupted without pH adjustment interventions, allowing the natural acidification to proceed continuously until the desired pH is reached. This eliminates the need for stopping and adjusting pH, maintaining continuous productive action.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The pH parameter changes naturally over time during cultivation due to metabolic activity, transitioning from initial pH to final pH of 5.5 or lower without external intervention. This temporal parameter change replaces the need for active pH control.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach minimizes polysaccharide modification and harmful substance generation, simplifying the production process while maintaining stringent protein and nucleic acid content specifications for vaccine production.

Implementation Method 1

cell lysis is carried out using a lysing agent such as sodium deoxycholate (DOC)

Methodology Applied
Scientific EffectCell lysis:

Implementation Method 2

protein precipitation by acidification of the cell lysate to a pH of less than 5.5

Methodology Applied
Scientific EffectProtein precipitation: Precipitation

Data Source

PatentEP2894225B1Production method for capsular polysaccharide having pneumococcal serotype
Publication Date: 2017.11.22 SK CHEMICALS CO LTD
  • EP2894225B1 patent drawingFigure 1
  • EP2894225B1 patent drawingFigure 2
  • EP2894225B1 patent drawingFigure 3

AI summary

The present invention provides an improved method of producing a capsular polysaccharide having a pneumococcal serotype. The method according to the present invention includes a step of additionally culturing bacterial cells producing a pneumococcal serotype without pH adjustment, thereby removing a protein precipitation process by acidification with a pH adjuster.