Nitrogen-Doped Carbon Catalyst for Durable Fuel Cell Electrodes

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Solution Overview

Problem

Existing carbon catalysts for fuel cells lack durability, and platinum-based catalysts are costly and scarce.

Innovation Solution

A carbon catalyst with specific nitrogen desorption characteristics, zeta potential isoelectric point, and nitrogen peak ratios in X-ray photoelectron spectroscopy is developed, enhancing durability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a carbon catalyst is used as an alternative to platinum catalyst, then cost is reduced and platinum reserves are conserved, but durability is insufficient

Engineering Contradiction:
Improvecatalyst durabilityVSAvoidcatalyst performance
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent applies parameter changes by precisely controlling the nitrogen desorption characteristics of the carbon catalyst. Specifically, it sets the nitrogen desorption amount in the 800-1000°C range to 0.75×10^-5 to 7.50×10^-5 mol/g and the zeta potential isoelectric point to pH 9.2 or higher. These parameter optimizations resolve the contradiction by achieving both durability and performance through controlled chemical properties rather than relying on expensive platinum materials.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite materials by creating a carbon catalyst with integrated nitrogen-containing functional groups embedded in the carbon structure. This composite approach combines the structural stability of carbon with the catalytic activity enhancement from nitrogen groups, achieving platinum-free durability through material composition optimization rather than using precious metals.

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If platinum catalyst is used in polymer electrolyte fuel cell, then catalytic performance is achieved, but cost increases and platinum reserves are depleted

Engineering Contradiction:
Improvecatalyst performanceVSAvoidplatinum usage
Core Design Contradiction:
Ease of manufactureVSQuantity of substance

Solution Approach 1:

The patent applies the extraction principle by removing platinum completely from the catalyst composition while retaining catalytic functionality through carbon-based materials with optimized nitrogen desorption characteristics. This eliminates dependency on platinum reserves and reduces cost, achieving the same performance through alternative material extraction from precious metal dependency.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses inexpensive carbon materials as substitutes for expensive platinum, creating a disposable-friendly catalyst that can be manufactured at low cost. The carbon catalyst with controlled nitrogen desorption properties provides sufficient durability for practical applications without requiring precious metals, enabling economical fuel cell production.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Reliability

If conventional carbon catalyst is used, then manufacturing is simple, but durability is poor

Engineering Contradiction:
Improvecatalyst durabilityVSAvoidcatalyst structure
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent resolves the simplicity-durability contradiction by optimizing specific parameters of the carbon catalyst structure. By controlling the nitrogen desorption amount (0.75×10^-5 to 7.50×10^-5 mol/g) and zeta potential isoelectric point (pH 9.2 or higher), the patent achieves enhanced durability without fundamentally changing the carbon catalyst manufacturing process, maintaining relative simplicity while improving performance through parameter precision.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The carbon catalyst exhibits improved durability, reducing the need for platinum and maintaining performance in fuel cell applications.

Implementation Method 1

a carbon structure that exhibits a nitrogen desorption amount in the temperature range from 800°C to 1, 000°C

Methodology Applied
Scientific EffectThermal desorption: Desorption

Implementation Method 2

a carbon structure that exhibits a zeta potential isoelectric point of pH 9.2 or more

Methodology Applied
Scientific EffectZeta potential: Electrostatics

Implementation Method 3

a ratio of an intensity of a first nitrogen peak that has a peak top within a range of a binding energy of 398.0±1.0 eV to an intensity of a second nitrogen peak that has a peak top within a range of a binding energy of 400.5±1.0 eV of 0.620 or more, the first nitrogen peak and the second nitrogen peak being obtained by separating a peak derived from a 1s orbital of a nitrogen atom in a photoelectron spectrum obtained by X-ray photoelectron spectroscopy

Methodology Applied
Scientific EffectPhotoelectric effect: Photoelectric Effect

Data Source

PatentEP3653297B1Carbon catalyst, battery electrode and battery
Publication Date: 2025.09.24 NISSHINBO HOLDINGS INC
  • EP3653297B1 patent drawingFigure 1
  • EP3653297B1 patent drawingFigure 2A
  • EP3653297B1 patent drawingFigure 2B

AI summary

Provided are a carbon catalyst, a battery electrode, and a battery, each having excellent durability. The carbon catalyst has: a carbon structure that exhibits a nitrogen desorption amount in the temperature range from 800°C to 1,000°C of 0.75×10-5 mol/g or more or a nitrogen desorption amount in the temperature range from 600°C to 1,000°Cof 1.20×10-5mol/g or more in a temperature programmed desorption method including measuring a nitrogen desorption amount in the temperature range from 600°C to 1,000°C; a carbon structure that exhibits a zeta potential isoelectric point of pH 9.2 or more; or a carbon structure that exhibits a ratio of an intensity of a first nitrogen peak that has a peak top within a range of a binding energy of 398.0±1.0 eV, to an intensity of a second nitrogen peak that has a peak top within a range of a binding energy of 400.5±1.0 eV, of 0.620 or more, the first nitrogen peak and the second nitrogen peak being obtained by separating a peak derived from a 1s orbital of a nitrogen atom in a photoelectron spectrum obtained by X-ray photoelectron spectroscopy.