Chiral Imaging Microscopy Using Structured Circular Polarization

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Solution Overview

Problem

Current methods for chiral imaging, such as direct wide-angle CD imaging, scanning CD confocal mapping, and chiral near-field scanning microscopy, face limitations including poor contrast, slow image acquisition, and low spatial resolution, making real-time chiral domain imaging impossible and unsuitable for high-resolution, subwavelength imaging of chiral samples.

Innovation Solution

The microscopy arrangement and method utilize structured illumination with optical chirality, where the light source is structured into alternating left and right circularly polarized light areas, enabling the moiré effect to enhance imaging resolution beyond the diffraction limit by superimposing the chiral structure of the illumination and the sample, allowing for rapid and high-resolution imaging of chiral domains with subwavelength spatial resolution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If direct wide-angle CD imaging or confocal CD mapping is used, then chiral imaging is achieved, but image acquisition time is long (up to 10 minutes) and real-time imaging is impossible

Engineering Contradiction:
Improvechiral domain imaging capabilityVSAvoidimage acquisition time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent employs periodic modulation of circularly polarized light handedness combined with lock-in detection to rapidly extract chiral signal information. By modulating the illumination at a specific frequency and detecting at that same frequency, the system achieves fast chiral imaging without requiring long integration times, thus enabling real-time imaging while maintaining measurement precision.

Inventive Principle:
Principle #19Periodic action

2Measurement precision

If scanning methods (confocal CD mapping, NSOM) are used, then chiral domain information is obtained, but image acquisition speed is slow and throughput is low

Engineering Contradiction:
Improvechiral domain spatial distributionVSAvoidimage acquisition speed
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The patent divides the illumination into multiple spatial channels using a spatial light modulator, allowing parallel acquisition of chiral information from different regions of the sample. This segmentation of the imaging process into simultaneous multi-point measurements eliminates the need for sequential scanning, dramatically increasing image acquisition speed while maintaining spatial distribution information.

Inventive Principle:
Principle #1Segmentation

3Measurement precision

If conventional optical microscopy is used, then imaging is achieved, but spatial resolution is diffraction-limited and subwavelength resolution is not possible

Engineering Contradiction:
Improvespatial resolutionVSAvoidimaging system requirements
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent replaces conventional mechanical scanning and diffraction-limited optical focusing with a spatial light modulator that uses computational algorithms to synthesize subwavelength focal spots. This substitution of mechanical/optical limiting factors with programmable light control enables super-resolution imaging without requiring complex mechanical systems or specialized optics.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

4Measurement precision

If chiral mapping methods (SHG, TPL) are used, then spatial resolution is improved, but sample requirements are restrictive (ordered mesoscopic structures) and contrast is reduced

Engineering Contradiction:
Improvespatial resolutionVSAvoidsample type applicability
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent changes the fundamental measurement parameter from nonlinear optical signals (SHG, TPL) to linear circular dichroism measurements. This parameter change allows the system to work with a broad range of sample types including disordered chiral structures, while maintaining high spatial resolution through spatial light modulator technology and achieving good contrast through lock-in detection of the circular dichroism signal.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables rapid and high-resolution imaging of chiral domains with subwavelength spatial resolution, overcoming the limitations of existing methods by combining optical chirality technology with structured illumination microscopy, suitable for various chiral biological objects and applications in drug design, macromolecules, and inorganic nanostructures.

Implementation Method 1

One physical property in which enantiomers differ is their interaction with linearly polarized light. The plane of linearly polarized light is rotated when passing through a solution of one enantiomer. This behavior is called optical activity.

Methodology Applied
Scientific EffectOptical activity: Polarisation

Implementation Method 2

enabling the moiré effect to enhance imaging resolution beyond the diffraction limit by superimposing the chiral structure of the illumination and the sample

Methodology Applied
Scientific EffectMoiré effect: Moiré Effect

Implementation Method 3

Chiral objects with opposite handedness also interact differently with circularly polarized light (CPL), resulting in circular birefringence and circular dichroism (CD).

Methodology Applied
Scientific EffectCircular birefringence: Birefringence

Implementation Method 4

Chiral objects with opposite handedness also interact differently with circularly polarized light (CPL), resulting in circular birefringence and circular dichroism (CD).

Methodology Applied
Scientific EffectCircular dichroism: Absorption (EM radiation)

Data Source

PatentEP3994515B1Microscopy arrangement and microscopy method for large-area, high-resolution chiral imaging, and use of same
Publication Date: 2024.07.31 LEIBNIZ INST FUR PHOTONISCHE TECHNOLOGIEN EV
  • EP3994515B1 patent drawingFigure 1
  • EP3994515B1 patent drawingFigure 2
  • EP3994515B1 patent drawingFigure 3

AI summary

The invention relates to a microscopy arrangement and a microscopy method for large-area, high-resolution chiral imaging, and use of same. The problem, which is addressed by the present invention, of providing a microscopy arrangement and microscopy method for large-area, high-resolution chiral imaging which quickly images chiral domains using subwavelength superresolution is solved in that, in order to image chiral samples, the optical chirality of the illumination is structured by the use of optical chirality and structured illumination microscopy in order to achieve extensive, high-resolution chiral imaging by using and evaluating optical magnification achieved by the moiré effect.