CMP Slurry with Accelerators for Silicon Nitride and Polysilicon Removal

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current chemical mechanical polishing slurries for silicon nitride and polysilicon in semiconductor manufacturing often lack selectivity, particularly in emerging technologies that require non-selective high removal rates for both materials, which are scarce in the market.

Innovation Solution

An acid chemical mechanical polishing slurry containing low concentration abrasive particles and specific compounds such as pyridine, piperidine, pyrrolidine, pyrrole, and pyrimidine derivatives with carboxyl or amino groups, along with silica abrasive particles and accelerating agents, to enhance the removal rates of silicon nitride and polysilicon.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional polishing slurry is used to achieve high removal rate of silicon nitride, then the removal rate of polysilicon also increases, but selectivity is lost

Engineering Contradiction:
Improveremoval rate of silicon nitrideVSAvoidselectivity between silicon nitride and polysilicon
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent changes the chemical parameters of the polishing slurry by introducing specific accelerators (pyridine, piperidine, pyrrolidine, pyrrole compounds with carboxyl groups and pyrimidine compounds with amino groups) and adjusting pH to 2-6. These parameter changes enable high removal rates of silicon nitride while maintaining selectivity against polysilicon, resolving the contradiction between productivity and manufacturing precision.

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If selective polishing slurry is used for silicon dioxide with low silicon nitride removal, then silicon nitride barrier layer is preserved, but high removal rate of silicon nitride is not achieved

Engineering Contradiction:
Improveselectivity of silicon dioxide to silicon nitrideVSAvoidremoval rate of silicon nitride
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent applies parameter changes by modifying the chemical composition with specific accelerators and pH adjustment to achieve non-selective high removal rates for both silicon nitride and polysilicon, which was previously scarce in the market.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite material approach by combining silica abrasive particles with organic accelerators (pyridine, piperidine, pyrrolidine, pyrrole, pyrimidine compounds) to create a polishing slurry that achieves high removal rates for multiple materials simultaneously.

Inventive Principle:
Principle #40Composite materials

3Productivity

If high concentration abrasive particles are used to increase removal rate, then polishing speed increases, but slurry viscosity and complexity increase

Engineering Contradiction:
Improvepolishing removal rateVSAvoidslurry concentration and viscosity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent changes the concentration parameter of abrasive particles to low levels (1-15% mass percent) while introducing organic accelerators to maintain high removal rates. This resolves the contradiction by achieving high productivity without increasing slurry complexity or viscosity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The slurry significantly increases the removal rates of both silicon nitride and polysilicon, achieving improved polishing performance across various semiconductor processes by adjusting the concentration of these compounds and maintaining a pH range of 2-6.

Implementation Method 1

silica abrasive particles

Methodology Applied
Scientific EffectAbrasion: Abrasion

Implementation Method 2

one or more compounds selected from pyridine compound, piperidine compound, pyrrolidine compound or pyrrole compound and their derivatives, which have one or more carboxyl groups, and pyrimidine compound having one or more amino groups

Methodology Applied
Scientific EffectChemical etching: Chemical Bonding

Data Source

PatentUS11898063B2Chemical-mechanical polishing solution
Publication Date: 2024.02.13 ANJI MICROELECTRONICS (SHANGHAI) CO LTD

AI summary

The present invention discloses a chemical mechanical polishing slurry, and the chemical mechanical polishing slurry comprises silica abrasive particles and accelerating agents, wherein the accelerating agents are selected from pyridine compound, piperidine compound, pyrrolidine compound or pyrrole compound and their derivatives, which have one or more carboxyl groups, and pyrimidine compound and its derivatives, which have one or more amino groups. The chemical mechanical polishing slurry can simultaneously increase the removal rate of both silicon nitride and polysilicon.