Copper-Ceria Catalyst for Selective Oxychlorination

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Solution Overview

Problem

Existing oxychlorination processes for hydrocarbons face challenges in controlling selectivity and minimizing byproducts such as carbon monoxide and carbon dioxide, which affects the efficiency and cost-effectiveness of the process.

Innovation Solution

A catalyst system comprising copper, cerium oxide (CeO2) as the carrier with 80 wt.% or more, and co-catalysts like alkali metals and lanthanide metals, which enhances catalytic stability and selectivity, reducing byproduct formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If high temperature pyrolysis of methane by chlorine is used, then the reaction can proceed, but lots of byproducts such as methylene chloride or cokes are generated and selectivity is poor

Engineering Contradiction:
Improvereaction rateVSAvoidbyproducts
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the reaction parameters by introducing a specific catalyst system (copper-based with alkali metal and lanthanide metal) that enables the oxychlorination reaction to proceed at lower temperatures with higher selectivity, avoiding the need for high temperature pyrolysis that generates harmful byproducts

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a catalyst as an intermediary substance that mediates the reaction between methane and chlorine. The catalyst system (copper, alkali metal, and lanthanide metal) provides an alternative reaction pathway that produces target products with high selectivity while minimizing harmful byproducts, effectively resolving the contradiction between reaction rate and byproduct formation

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of manufacture

If simple heating method is used for oxychlorination, then the process is simple, but control of selectivity is difficult and byproducts are generated

Engineering Contradiction:
Improveprocess simplicityVSAvoidselectivity control
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent introduces a catalyst system as an intermediary that enables precise control of selectivity while maintaining process simplicity. The catalyst (copper-based with alkali metal and lanthanide metal) provides specific active sites that direct the reaction toward desired products, allowing selective control without complicating the overall process

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If conventional catalysts are used, then the process can run, but catalytic stability is insufficient and byproducts like carbon monoxide and carbon dioxide are produced

Engineering Contradiction:
Improvecatalytic stabilityVSAvoidcarbon monoxide and carbon dioxide
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent employs a composite catalyst system comprising copper, alkali metal, and lanthanide metal components. This composite structure enhances catalytic stability and specificity, enabling the catalyst to maintain high performance over time while selectively promoting the formation of desired oxychlorination products and minimizing harmful byproducts like carbon monoxide and carbon dioxide

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst system increases the selectivity of target products like chloromethane while suppressing the production of carbon monoxide and carbon dioxide, even at lower temperatures, thereby improving process efficiency and reducing costs.

Implementation Method 1

a catalyst for an oxychlorination process of hydrocarbons, the catalyst including: a catalyst material including copper; and a carrier including cerium oxide (CeO2)

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3721993B1Catalyst for processing oxychlorination of hydrocarbon, preparation method therefor, and preparation method of oxychlorinated compound of hydrocarbon using same
Publication Date: 2022.06.15 LG CHEM LTD
  • EP3721993B1 patent drawingFigure 1
  • EP3721993B1 patent drawingFigure 2
  • EP3721993B1 patent drawingFigure 3

AI summary

The present specification provides a catalyst for an oxychlorination process of hydrocarbons, a preparation method thereof, and a method for preparing an oxychlorination compound of hydrocarbons using the same.