Enamel Microcrack Resistance Evaluation for Oral Care Compositions

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Solution Overview

Problem

Enamel micro-cracks and microscratches are common and lead to enamel weakening, increased staining, and tooth wear, with existing treatments focusing on chemical changes rather than physical damage, necessitating improved physical protection and remineralization methods.

Innovation Solution

A method to evaluate and enhance enamel micro-crack and microscratch resistance by generating controlled fractures and scratches on enamel samples, measuring mechanical properties, and treating with oral care compositions to assess their efficacy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If chemical treatments are used to address enamel issues, then remineralization is improved, but physical damage resistance is insufficient

Engineering Contradiction:
Improveenamel remineralizationVSAvoidenamel micro-crack resistance
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent applies composite materials by combining chemical remineralization agents with physical reinforcement substances. The composition includes both chemical components (fluoride, calcium, phosphate) and physical reinforcement particles (silica, hydroxyapatite, glass ions) that work synergistically to provide both remineralization and mechanical strength enhancement to the enamel.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent utilizes parameter changes by modifying the physical and chemical properties of enamel through controlled treatment. The method changes parameters such as mineral density, micro-hardness, and micro-crack resistance through application of compositions with specific concentrations of active ingredients, transforming the enamel's mechanical properties to resist physical damage while maintaining remineralization.

Inventive Principle:
Principle #35Parameter changes

2Strength

If enamel is treated to reduce micro-cracks, then fracture toughness is improved, but brittleness remains high in older teeth

Engineering Contradiction:
Improvefracture toughnessVSAvoidenamel brittleness
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent applies local quality by providing targeted treatment to specific enamel regions affected by micro-cracks and wear. The composition is applied locally to areas showing signs of damage, allowing differential treatment that enhances fracture toughness in compromised areas while maintaining overall enamel integrity, addressing the specific needs of older teeth with higher brittleness.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent utilizes preliminary action by applying the composition before physical damage occurs or progresses. The treatment is applied proactively to prevent micro-crack formation and propagation, particularly in older teeth that are more brittle, thereby preemptively improving fracture toughness before significant damage occurs.

Inventive Principle:
Principle #10Preliminary action

3Strength

If physical protection methods are implemented, then micro-crack resistance is improved, but staining resistance is insufficient

Engineering Contradiction:
Improveenamel micro-crack resistanceVSAvoidenamel staining
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent applies composite materials by incorporating both physical reinforcement agents (silica particles, hydroxyapatite) and chemical staining resistance components (fluoride, zinc compounds) in a single composition. This composite approach simultaneously provides mechanical strength enhancement through physical particles and staining resistance through chemical agents, resolving the contradiction between physical protection and staining prevention.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent utilizes universality by designing a multi-functional composition that addresses multiple enamel concerns simultaneously. The single treatment composition provides both physical protection against micro-cracks and chemical protection against staining, eliminating the need for separate treatments and achieving both objectives with one application.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Strength

If enamel is protected from physical damage, then microscratch resistance is improved, but wear resistance decreases with age

Engineering Contradiction:
Improvemicroscratch resistanceVSAvoidenamel wear resistance
Core Design Contradiction:
StrengthVSDuration of action of stationary object

Solution Approach 1:

The patent applies preliminary action by treating the enamel before significant wear occurs, particularly in older teeth. The composition is applied periodically to maintain and enhance microscratch resistance and wear resistance over time, counteracting the natural aging process that increases susceptibility to wear and preventing progressive enamel degradation.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent utilizes continuity of useful action by implementing ongoing treatment protocols that maintain enamel protection throughout the tooth's lifespan. The composition is applied repeatedly over time to sustain microscratch and wear resistance, ensuring continuous protection against physical damage as the tooth ages and becomes more vulnerable to wear.

Inventive Principle:
Principle #20Continuity of useful action

Data Source

PatentUS12517024B2Method of evaluating the enamel microcrack resistance efficacy of compositions
Publication Date: 2026.01.06 COLGATE PALMOLIVE CO
  • US12517024B2 patent drawing
  • US12517024B2 patent drawing

AI summary

Disclosed are methods of determining enamel micro-crack and/or microscratch resistance and also methods of identifying compositions that are effective in increasing enamel micro-crack and/or microscratch resistance or evaluating the efficacy of compositions in increasing enamel micro-crack and/or microscratch resistance.