Ferromagnetic Substrate Graphene Synthesis Without Vacuum

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Solution Overview

Problem

Existing methods for graphene and carbon nanomaterial synthesis require vacuum conditions, expensive substrates like nickel or copper, and are energy-intensive, limiting the use of ferromagnetic materials and carbon precursors.

Innovation Solution

A method utilizing electromagnetic induction to heat a ferromagnetic substrate in ambient atmosphere, igniting a carbon precursor to consume oxygen, allowing carbon atoms to diffuse and form graphene clusters on the substrate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If vacuum conditions and expensive substrates like nickel or copper are used for graphene synthesis, then synthesis quality is improved, but substrate cost and equipment complexity increase

Engineering Contradiction:
Improvesynthesis qualityVSAvoidequipment complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The invention extracts the essential function of vacuum conditions and reduces it to ambient atmosphere operation. By removing the vacuum requirement while maintaining graphene synthesis quality, the system eliminates complex vacuum equipment and achieves the same synthesis outcome in simpler ambient conditions.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention replaces expensive, traditional substrates like nickel or copper with inexpensive ferromagnetic substrates. These cheaper substrates achieve comparable synthesis results, eliminating the need for costly material resources while maintaining synthesis quality.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Temperature

If traditional heating methods are used for graphene synthesis, then substrate heating is achieved, but energy consumption and processing time increase

Engineering Contradiction:
Improvesubstrate heatingVSAvoidenergy consumption
Core Design Contradiction:
TemperatureVSUse of energy by moving object

Solution Approach 1:

The invention replaces traditional thermal heating methods with electromagnetic induction heating. This substitution uses electromagnetic fields to directly induce currents in the ferromagnetic substrate, generating heat internally and rapidly achieving the required temperature with significantly reduced energy consumption and shorter processing time.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Quantity of substance

If high carbon solubility metals like iron or steel are used as substrates, then carbon diffusion is improved, but oxygen elimination becomes problematic in ambient atmosphere

Engineering Contradiction:
Improvecarbon diffusionVSAvoidoxygen interference
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The invention performs preliminary oxygen elimination by igniting the carbon precursor to consume atmospheric oxygen before the main synthesis process begins. This preliminary action creates an oxygen-depleted environment that allows subsequent carbon diffusion into the ferromagnetic substrate without oxidation interference, enabling the use of high carbon solubility metals.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention converts the harmful effect of atmospheric oxygen into a beneficial process by using the carbon precursor combustion to consume oxygen. The same carbon precursor that would otherwise be a simple carbon source becomes an oxygen-removing agent, transforming the ambient atmosphere from a harmful oxidizing environment into a beneficial carbon-supplying environment.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables faster, more energy-efficient graphene synthesis using any ferromagnetic substrate and precursor, reducing energy consumption and substrate costs.

Implementation Method 1

the substrate is heated up by electromagnetic induction

Methodology Applied
Scientific EffectElectromagnetic induction: Electromagnetic Induction

Implementation Method 2

the carbon precursor is ignited. 5) at the end of combustion, when the flame goes out due to lack of oxygen

Methodology Applied
Scientific EffectCombustion: Combustion

Implementation Method 3

the substrate and thermally decomposing the organic precursor; 5) at the end of combustion, when the flame goes out due to lack of oxygen, heating of the carbon precursor continues until it evaporates or thermally decomposes

Methodology Applied
Scientific EffectThermal decomposition: Pyrolysis

Implementation Method 4

gases produced by the carbon precursor come into contact with the hot substrate; The carbon atoms diffused in the substrate come to the surface and form graphene clusters

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentUS12473634B2Method for synthesis of graphene and other carbon nanomaterials on a ferromagnetic substrate in the ambient atmosphere
Publication Date: 2025.11.18 KALNINS VIESTURS
  • US12473634B2 patent drawing

AI summary

The presented invention relates to the graphene and other carbon nanomaterial synthesis which requires a metal substrate-catalyst, elevated temperature and carbon precursors. The method for the synthesis of graphene and other carbon nanomaterials on a ferromagnetic substrate in the ambient atmosphere includes the following steps: 1) introducing a ferromagnetic substrate into a closed chamber having an ambient atmosphere; 2) applying a carbon precursor to said substrate; 3) heating the substrate by electromagnetic induction, whereby the carbon precursor is evaporated and/or thermally decomposed; 4) igniting the carbon precursor; 5) cooling the substrate. The carbon precursor can be a single chemical or a mixture of various different carbon precursors.