Graphene Pinhole-Blocking Layer for X-Ray Radiation Windows

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Solution Overview

Problem

Existing radiation window materials for X-ray applications often suffer from pinholes, leading to gas leakage and contamination in gas-filled enclosures, and mechanical stress issues due to pressure differences.

Innovation Solution

A radiation window membrane is created using a graphene pinhole-blocking layer attached to a window base layer, where the graphene layer is produced using thin film manufacturing techniques like CVD or ALD to prevent pinholes and enhance mechanical properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If thin film manufacturing techniques (sputtering or chemical vapor deposition) are used to create additional layers on a beryllium base membrane, then X-ray transmission is improved, but pinholes may appear causing gas leakage

Engineering Contradiction:
Improvegas tightnessVSAvoidpinhole-free quality
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent uses a graphene layer (a single-atom-thick film) as a pinhole-blocking layer on the beryllium membrane. This ultra-thin film structure effectively seals pinholes while maintaining X-ray transmission, as graphene's two-dimensional continuous structure blocks gas leakage pathways without significantly attenuating X-rays.

Inventive Principle:
Principle #30Flexible shells and thin films

Solution Approach 2:

The patent creates a composite structure by combining beryllium base membrane with a graphene pinhole-blocking layer. This composite material leverages the advantages of both materials: beryllium provides good X-ray transmission and mechanical strength, while graphene provides pinhole sealing capability, together achieving both gas tightness and manufacturing feasibility.

Inventive Principle:
Principle #40Composite materials

2Reliability

If the window membrane is made thinner to reduce X-ray attenuation, then X-ray transmission is improved, but mechanical strength to withstand pressure difference deteriorates

Engineering Contradiction:
ImproveX-ray transmissionVSAvoidmechanical strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent employs an ultra-thin graphene layer as a reinforcement coating on the beryllium membrane. This atomically thin film significantly enhances the mechanical strength and pressure resistance of the membrane without appreciably increasing thickness, thereby maintaining excellent X-ray transmission while preventing membrane failure under pressure differential.

Inventive Principle:
Principle #30Flexible shells and thin films

Solution Approach 2:

The composite structure of beryllium base membrane plus graphene coating creates a material system where the graphene layer acts as a strength-enhancing reinforcement. This composite achieves superior mechanical properties compared to pure beryllium, enabling thinner designs that maintain both X-ray transmission and pressure withstand capability.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The graphene pinhole-blocking layer effectively prevents gas leakage and enhances the mechanical strength of the radiation window membrane, ensuring reliable X-ray transmission with minimal attenuation and improved durability.

Implementation Method 1

a pinhole-blocking layer on a surface of the window base layer, which pinhole-blocking layer comprises graphene

Methodology Applied
Scientific EffectPinhole-blocking:

Implementation Method 2

through which opening X-rays are to pass

Methodology Applied
Scientific EffectX-ray transmission: X-Ray

Data Source

PatentUS8494119B2Radiation window, and a method for its manufacturing
Publication Date: 2013.07.23 OXFORD INSTR TECH OY
  • US8494119B2 patent drawing
  • US8494119B2 patent drawing
  • US8494119B2 patent drawing

AI summary

A radiation window membrane and for covering an opening in an X-ray device is presented, as well a method for its manufacturing. Said openings are such through which X-rays are to pass. The membrane comprises a window base layer and a pinhole-blocking layer on a surface of said window base layer. Said pinhole-blocking layer comprises graphene.