Natural Graphite Anode Material for Low-Expansion Lithium Batteries

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Solution Overview

Problem

Natural graphite-based negative electrodes in lithium secondary batteries face significant cycle expansion issues due to electrolyte side reactions, limiting their capacity and lifespan despite their high output and capacity potential.

Innovation Solution

A negative electrode active material is developed using natural graphite with a D90/D10 ratio of 2.20 or less, a D50 of 6 μm to 11 μm, and a BET specific surface area of 2.2 m2/g or less, prepared through a Cold Isostatic Press method to reduce particle pores and enhance packing, combined with a carbon coating layer to prevent electrolyte side reactions and improve structural stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If natural graphite is used as negative electrode active material, then output and capacity are improved, but cycle expansion problem occurs due to electrolyte side reaction

Engineering Contradiction:
Improveoutput and capacityVSAvoidcycle expansion problem
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies parameter changes by controlling the particle size distribution parameters (D90/D10 ratio ≤ 2.20, D50 between 6-11 μm, BET specific surface area ≤ 2.2 m2/g) of natural graphite to resolve the contradiction between high output/capacity and cycle expansion prevention

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by combining natural graphite with artificial graphite in specific ratios to create a negative electrode active material that maintains the high output and capacity of natural graphite while reducing cycle expansion through the structural stability of artificial graphite

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If natural graphite is used to achieve high capacity, then battery energy density is improved, but thickness expansion occurs during charging and discharging

Engineering Contradiction:
ImprovecapacityVSAvoidthickness expansion
Core Design Contradiction:
Quantity of substanceVSVolume of moving object

Solution Approach 1:

The patent controls the particle size distribution parameters (D90/D10 ratio ≤ 2.20, D50 between 6-11 μm) to optimize packing density and minimize volume expansion during lithium ion intercalation and deintercalation cycles

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies different particle size ranges to different portions of the electrode structure, using a controlled distribution where smaller particles fill voids between larger particles, optimizing both capacity and volume stability

Inventive Principle:
Principle #3Local quality

3Productivity

If natural graphite particles are reduced in size to improve packing, then capacity is improved, but specific surface area increases causing more electrolyte side reactions

Engineering Contradiction:
ImprovecapacityVSAvoidelectrolyte side reaction
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent optimizes the BET specific surface area parameter to ≤ 2.2 m2/g while maintaining high capacity through controlled particle size distribution (D50: 6-11 μm), balancing the trade-off between packing density and side reaction prevention

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent utilizes the natural porous structure of graphite particles with controlled surface area to enable efficient lithium ion transport while minimizing electrolyte contact and side reactions

Inventive Principle:
Principle #31Porous materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively prevents cycle expansion and thickness growth, maintaining high output and capacity properties while enhancing the lifespan of the battery by optimizing particle size distribution and surface area, thereby improving the battery's charging performance and structural integrity.

Implementation Method 1

a method for preparing a negative electrode active material, the method including a process of pressurizing natural graphite by a Cold Isostatic Press method

Methodology Applied
Scientific EffectCold Isostatic Pressing:

Implementation Method 2

a BET specific surface area is 2.2 m2/g or less

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentUS11881584B2Negative electrode active material, preparation method thereof, negative electrode and secondary battery both including same
Publication Date: 2024.01.23 LG ENERGY SOLUTION LTD

AI summary

A negative electrode active material including natural graphite, wherein a D90/D10, which is the ratio of D90 to D10, is 2.20 or less, a D50 is 6 μm to 11 μm, and a BET specific surface area is 2.2 m2/g or less.