HFO-1234yf Ethane Refrigerant Blend With Negligible Glide

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Solution Overview

Problem

The automotive and stationary refrigeration industries face challenges in finding low Global Warming Potential (GWP) refrigerants that can effectively provide both heating and cooling, especially at low temperatures, while also meeting requirements for low toxicity, low flammability, and negligible glide to facilitate efficient thermal management in hybrid, electric, and mass transport vehicles, as well as residential and commercial structures.

Innovation Solution

Development of azeotropic and near-azeotropic compositions of HFO-1234yf and ethane (R-170) that exhibit ultra-low GWP, low toxicity, and low flammability, with negligible temperature glide, enabling efficient thermal management systems for heating and cooling applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If R-134a is used as the automotive refrigerant, then cooling performance is maintained, but global warming potential is high and the refrigerant is being phased out

Engineering Contradiction:
Improveglobal warming potentialVSAvoidrefrigerant availability
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters by transitioning from HFC-based R-134a to an HFO-1234yf and ethane blend, achieving ultra-low GWP (less than 10) while maintaining refrigeration functionality. This parameter change resolves the contradiction by adopting a chemically different substance with improved environmental properties.

Inventive Principle:
Principle #35Parameter changes

2Weight of moving object

If ICE size is reduced or eliminated in electrified vehicles, then vehicle weight is reduced and electric drive-cycle is increased, but heating capability is compromised

Engineering Contradiction:
Improvevehicle weightVSAvoidpassenger cabin heating
Core Design Contradiction:
Weight of moving objectVSTemperature

Solution Approach 1:

The heat pump system using HFO-1234yf/ethane refrigerant performs both cooling and heating functions, replacing the ICE's secondary heating function. The system provides heating by reversing the refrigeration cycle, extracting heat from the environment and delivering it to the passenger cabin, thus achieving multi-functionality that resolves the heating capability loss.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Adaptability or versatility

If refrigerant blends with high glide are used, then composition flexibility is improved, but serviceability is degraded due to inability to reconstitute on-site

Engineering Contradiction:
Improvecomposition flexibilityVSAvoidserviceability
Core Design Contradiction:
Adaptability or versatilityVSEase of repair

Solution Approach 1:

The patent creates a near-azeotropic blend with less than 3K temperature glide, making the refrigerant composition extremely homogeneous in terms of phase change behavior. This near-homogeneity allows the refrigerant to function as a single-substance equivalent during service operations, enabling on-site recovery, recycling, and recharge without requiring complex reconstitution equipment or procedures.

Inventive Principle:
Principle #33Homogeneity

4Object-affected harmful factors

If low GWP refrigerants are developed, then environmental impact is reduced, but thermal management performance at low temperatures may be compromised

Engineering Contradiction:
Improveenvironmental impactVSAvoidlow temperature performance
Core Design Contradiction:
Object-affected harmful factorsVSTemperature

Solution Approach 1:

The patent uses a composite refrigerant blend of HFO-1234yf and ethane in specific proportions (at least 90 wt% HFO-1234yf and up to 10 wt% ethane). This composite composition combines the ultra-low GWP properties of HFO-1234yf with the thermodynamic properties of ethane to achieve both environmental compliance and effective heating performance down to -30°C.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The HFO-1234yf and ethane blends provide improved refrigeration capacity, extend the lower heating range capability, maintain low GWP and flammability, and exhibit negligible glide, making them suitable for electrified vehicles and other thermal management systems from -30°C to +40°C.

Implementation Method 1

The compositions exhibit azeotropic and near azeotropic behavior... low temperature glide (less than 3K) or nearly negligible glide (less than 0.75K)... capable of being used in the heating, and/or in the cooling mode

Methodology Applied
Scientific EffectPhase change: Phase Change

Data Source

PatentEP3861083B1Azeotropic composition of HFO-1234yf and ethane
Publication Date: 2024.03.20 THE CHEMOURS CO FC LLC
  • EP3861083B1 patent drawingFigure 1
  • EP3861083B1 patent drawingFigure 2
  • EP3861083B1 patent drawingFigure 3

AI summary

Refrigerant compositions including 2,3,3,3-tetrafluoropropene (HFO-1234yf) and at least one of ethane (R-170) or propane (R-290) which exhibit near-azeotropic or azeotrope-like behavior. The refrigerant compositions exhibit a low global warming potential (GWP) and are non-ozone depleting. The refrigerant compositions are useful as a heating or cooling fluids in a variety of heating or cooling systems including heat pumps and other heating and cooling loops, in, for example, the automotive industry.