Hot-Work Tool Steel Bainitization via Isothermal Holding

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Solution Overview

Problem

Conventional methods for producing hot-work steels face challenges in achieving bainitization within economically justifiable time frames, often requiring lengthy treatment processes that can lead to incomplete transformation and residual austenite formation.

Innovation Solution

A method involving austenitization followed by rapid cooling to a holding temperature between 330°C and 360°C, with isothermal holding until bainitization is complete, allowing for measurement of the transformation using dilatometers to ensure complete bainite formation without residual austenite, and subsequent cooling to room temperature.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If conventional heat treatment methods are used for bainitization, then complete transformation to bainite structure is achieved, but the treatment time becomes excessively long and economically unjustifiable

Engineering Contradiction:
Improvebainite structure completenessVSAvoidtreatment time
Core Design Contradiction:
Stability of the object's compositionVSLoss of time

Solution Approach 1:

The invention modifies the chemical composition parameters of the steel by adding boron (0.0005-0.005 wt%) and optimizing alloying elements (Cr: 1.5-4.0 wt%, Mo: 0.5-2.0 wt%, B: 0.0005-0.005 wt%). These parameter changes shift the transformation kinetics, enabling complete bainitization within 2-8 hours at 330-360°C, thus resolving the contradiction between transformation completeness and treatment time

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite microstructure consisting of bainite as the primary phase with controlled residual austenite (3-15%) and minimal martensite (<5%). This composite approach at the microstructural level achieves both complete transformation and acceptable treatment time by leveraging the synergistic effects of different phases

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If rapid cooling is applied to achieve complete austenite transformation, then residual austenite is minimized, but the cooling rate requirements become difficult to control and may result in incomplete transformation

Engineering Contradiction:
Improveresidual austenite contentVSAvoidcooling control difficulty
Core Design Contradiction:
Stability of the object's compositionVSEase of manufacture

Solution Approach 1:

By adding boron and optimizing alloy composition, the invention changes the transformation temperature and kinetics parameters. This allows the use of moderate cooling rates (0.5-5°C/s) that are easier to control while still achieving complete austenite transformation and minimizing residual austenite to 3-15%

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs dilatometric measurement during the heat treatment process to monitor the transformation progress in real-time. This feedback mechanism allows for dynamic adjustment of holding time and temperature to ensure complete transformation while avoiding excessive residual austenite, making the process more controllable

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables a completely bainitic structure to be achieved in a technically reasonable time, with improved mechanical properties and reduced thermal expansion, allowing for adjustable strength through tempering, while avoiding residual austenite and martensite formation.

Implementation Method 1

austenitization followed by rapid cooling to a holding temperature between 330°C and 360°C

Methodology Applied
Scientific EffectAustenitization: Phase Change

Implementation Method 2

cooling the steel after an austenitizing treatment to a holding temperature and keeping it at this holding temperature until the bainitization is complete

Methodology Applied
Scientific EffectBainitization: Phase Change

Implementation Method 3

measurement of the transformation using dilatometers to ensure complete bainite formation

Methodology Applied
Scientific EffectDilatometry:

Implementation Method 4

allowing for adjustable strength through tempering

Methodology Applied
Scientific EffectTempering: Heat Treatment

Data Source

PatentEP3332040B1Method for producing a tool steel
Publication Date: 2021.03.03 VOESTALPINE BOEHLER EDELSTAHL GMBH & CO KG
  • EP3332040B1 patent drawingFigure 1
  • EP3332040B1 patent drawingFigure 2
  • EP3332040B1 patent drawingFigure 3

AI summary

Method for producing a tool steel, in particular a hot-work tool steel, characterized in that a steel of the following analysis: C: 0.25 - 0.6% by weight; Si: max. 0.15% by weight; Mn: max. 0.3% by weight; Mo: 2 - 5% by weight; Cr: 0 - 2% by weight; W: 1 - 3% by weight; V: 0 - 2% by weight; Ni: 0 - 3% by weight, the remainder iron and melting-induced unavoidable impurities is melted and alloyed, wherein a workpiece of the steel is heated up and austenitized at temperatures &gt; Ac3 and subsequently cooled down, wherein the cooling is performed to a temperature of 330°C to 360°C and the workpiece is kept isothermally at this temperature until the workpiece has been completely bainitically transformed, and subsequently the cooling is performed to room temperature, and also a hot-work tool steel for this and use thereof.