Hydrogen-Enriched Nb-Ti Hairspring for Thermal Stability

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Solution Overview

Problem

Existing watchmaking spiral springs made from binary NB-Ti alloys face challenges in maintaining low secondary error and thermal coefficient while ensuring chronometric performance across varying temperatures.

Innovation Solution

A spiral spring manufactured from a niobium, titanium, and hydrogen alloy, where hydrogen is added through thermochemical treatment under controlled atmosphere, resulting in a microstructure with a single beta phase and hydrogen mainly in the form of interstitials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If binary Nb-Ti alloy is used to achieve low thermal coefficient, then thermal coefficient is improved, but secondary error worsens

Engineering Contradiction:
Improvethermal coefficientVSAvoidsecondary error
Core Design Contradiction:
TemperatureVSManufacturing precision

Solution Approach 1:

The patent uses a composite microstructure consisting of two distinct phases: a beta phase matrix and alpha phase precipitates. This composite structure allows the material to simultaneously achieve low thermal coefficient (through the beta phase) and low secondary error (through the alpha phase precipitates), resolving the contradiction between these two performance parameters.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention introduces localized alpha phase precipitates within the beta phase matrix. These precipitates are distributed specifically within the alloy structure to correct the secondary error, while the overall beta phase structure maintains the low thermal coefficient. This local modification approach allows independent optimization of different performance characteristics.

Inventive Principle:
Principle #3Local quality

2Manufacturing precision

If binary Nb-Ti alloy is used to achieve low secondary error, then secondary error is improved, but thermal coefficient worsens

Engineering Contradiction:
Improvesecondary errorVSAvoidthermal coefficient
Core Design Contradiction:
Manufacturing precisionVSTemperature

Solution Approach 1:

The patent employs a composite microstructure with beta phase matrix and alpha phase precipitates. The beta phase provides low thermal coefficient while the alpha phase precipitates provide low secondary error, achieving both performance targets simultaneously through material composition design.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention changes the microstructural parameters of the alloy by controlling the size, distribution, and volume fraction of alpha phase precipitates within the beta phase matrix. By adjusting these microstructural parameters through heat treatment and alloy composition, both thermal coefficient and secondary error are optimized to acceptable ranges.

Inventive Principle:
Principle #35Parameter changes

3Temperature

If alloy composition is optimized for low thermal coefficient, then thermal coefficient is improved, but breaking load worsens

Engineering Contradiction:
Improvethermal coefficientVSAvoidbreaking load
Core Design Contradiction:
TemperatureVSStrength

Solution Approach 1:

The patent creates a composite microstructure where alpha phase precipitates are distributed within the beta phase matrix. This composite structure simultaneously achieves low thermal coefficient and high breaking load, as the alpha phase precipitates act as reinforcement that strengthens the material while the beta phase maintains the desired thermal properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention introduces localized alpha phase precipitates that provide strengthening effect in specific regions of the alloy. These precipitates are strategically distributed to enhance breaking load without significantly affecting the overall thermal coefficient, which is primarily determined by the beta phase matrix composition.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves a secondary error close to zero and a thermal coefficient close to zero, while maintaining a high charge at rupture (RM) and elasticity module, thereby enhancing the chronometric performance and stability of the spiral spring across temperature variations.

Implementation Method 1

hydrogen is added to the Nb-Ti alloy by thermochemical treatment under a controlled atmosphere during the manufacturing process

Methodology Applied
Scientific EffectThermochemical treatment:

Implementation Method 2

The spiral spring thus produced contains hydrogen mainly or exclusively in the form of interstitials

Methodology Applied
Scientific EffectInterstitial absorption: Absorption (physical)

Data Source

PatentEP4123393B1Hairspring for clock movement
Publication Date: 2025.04.16 NIVAROX FAR SA
  • EP4123393B1 patent drawingFigure 1~2
  • EP4123393B1 patent drawingFigure 3~4
  • EP4123393B1 patent drawingFigure 5

AI summary

The present invention relates to a balance spring for use in a clockwork movement, characterized in that the balance spring is made of an alloy consisting of: - Nb, Ti, H, and possible traces of other elements selected from O, C, Fe, N, Ni, Si, Cu, and Al, with the following weight percentages: - a Ti content between 1 and 80%, - an H content between 0.17 and 2%, - a total content for all other elements less than or equal to 0.3% by weight, - the remaining 100% being Nb. The present invention also relates to its manufacturing process, comprising a thermochemical treatment step of a blank made of an Nb-Ti alloy in an atmosphere containing hydrogen, so as to enrich the Nb-Ti alloy with hydrogen in the form of interstitials.