Gas-Phase Hydrogen Permeation Test Device Safety

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Solution Overview

Problem

Current methods cannot safely measure hydrogen permeation behavior in materials under ultra-high-pressure hydrogen environments, such as those found in hydrogen fuel cell vehicle systems, due to the risk of explosion and equipment damage from pressure differences and potential leaks.

Innovation Solution

A gas-phase hydrogen permeation test device that uses a high-pressure hydrogen feeder, analyzer, and safety valves to manage pressure and prevent explosions, with a passive discharger to safely release hydrogen in case of test piece failure, allowing for safe measurement of hydrogen permeation in materials under high-pressure conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If high-pressure hydrogen gas is used for permeation testing, then measurement precision is improved, but safety deteriorates due to explosion risk

Engineering Contradiction:
Improvehydrogen permeation measurement precisionVSAvoiddevice safety
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The device is divided into two separate chambers: a high-pressure hydrogen atmosphere chamber for applying hydrogen pressure to the test piece, and a reduced-pressure analysis chamber for detecting permeated hydrogen. This segmentation allows each chamber to be optimized for its specific function while isolating safety risks to the controlled high-pressure zone.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A passive discharger (safety valve or rupture disc) is installed as an intermediary safety device in the secondary-side pipe. This passive protection mechanism automatically activates when pressure exceeds safe limits, providing a fail-safe release path for hydrogen gas without requiring active control systems.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 3:

The high-pressure chamber is designed as an explosion-proof environment that can safely contain hydrogen gas at ultra-high pressures (up to 82 MPa). The chamber construction and ventilation systems create a controlled inert environment that prevents hydrogen from reaching explosive concentrations.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Adaptability or versatility

If ultra-high-pressure hydrogen environment is created, then adaptability is improved, but device complexity increases due to safety requirements

Engineering Contradiction:
Improvepressure environment adaptabilityVSAvoidsafety system complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The passive discharger is pre-installed in the secondary-side pipe before testing begins. This preliminary safety measure ensures that if pressure builds up beyond safe limits during testing, the discharger will automatically activate without requiring real-time monitoring or intervention, simplifying the control system while maintaining safety.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The passive discharger operates autonomously based on pressure conditions alone, without requiring external control signals or power sources. The safety valve or rupture disc self-activates when pressure exceeds its design threshold, providing a simple, reliable safety mechanism that does not add complexity to the control system.

Inventive Principle:
Principle #25Self-service

3Productivity

If pressure difference is increased for permeation testing, then productivity is improved, but harmful factors increase due to potential leaks

Engineering Contradiction:
Improvetesting efficiencyVSAvoidleakage risk
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The passive discharger converts the potential harmful effect of pressure buildup into a beneficial safety feature. By designing the system with a predetermined pressure release mechanism, any pressure excess that could lead to dangerous leaks is automatically converted into a controlled, safe discharge of hydrogen gas through the discharger.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables safe investigation of hydrogen permeation behavior in materials under high-pressure hydrogen atmospheres, preventing device damage and explosion risks, and allowing for the evaluation of materials' performance at pressures up to 82 MPa.

Implementation Method 1

a passive discharger provided in the secondary-side pipe; either or both of (i) a safety valve which is configured to be placed into an open state when the pressure inside the secondary-side pipe reaches or exceeds a specific value, and provide communication between the inside and outside of the secondary-side pipe, and (ii) a rupture disc which is configured to rupture when the pressure inside the secondary-side pipe reaches or exceeds a specific value, and provide communication between the inside and outside of the secondary-side pipe

Methodology Applied
Scientific EffectPressure relief: Pressure Gradient

Implementation Method 2

hydrogen permeation behavior in a material under an ultra high-pressure hydrogen environment as high as 82 MPa, for example, which is the pressure of the pressure vessel under consideration for practical application. (1) Hydrogen itself, in its nature, can extremely easily cause an explosion

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP3273220B1Gas-phase hydrogen permeation test device and method of protecting gas-phase hydrogen permeation test device
Publication Date: 2021.09.08 JFE STEEL CORP
  • EP3273220B1 patent drawingFigure 1

AI summary

Provided is a gas-phase hydrogen permeation test device capable of safely measuring hydrogen permeation behavior in a material under a high-pressure hydrogen atmosphere. The gas-phase hydrogen permeation test device includes a high-pressure hydrogen feeder, an analyzer, a primary-side pipe, a secondary-side pipe, a secondary-side pressure gauge, a primary-side shut-off valve, a primary-side discharge valve, a secondary-side discharge valve, a passive discharger, a secondary-side shut-off valve, and a controller configured to, when the pressure measured by the secondary-side pressure gauge reaches or exceeds a specific value, place the primary-side shut-off valve and the secondary-side shut-off valve into a closed state and the primary-side discharge valve and the secondary-side discharge valve into an open state, in which the primary-side shut-off valve, the primary-side discharge valve, and the secondary-side discharge valve are air-operated valves, the passive discharger is either or both of a safety valve and a rupture disk, the high-pressure hydrogen feeder, the primary-side pipe, the primary-side shut-off valve, the primary-side discharge valve, the passive discharger, the test piece, and the secondary-side discharge valve are installed in an explosion-proof environment, and the analyzer is installed in a non-explosion-proof environment.